Preparation and use method of waterproof coating agent of outdoor exercise rope
A waterproof coating and rope technology, which is applied in the field of rope nets, can solve the problems of nylon fibers such as easy moisture absorption, reduced strength, and reduced wear resistance, and achieves simple production processes and usage methods, good water repellency, and low surface area. The effect of the tension value
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preparation example Construction
[0025] A preparation method of an outdoor sports rope waterproof coating agent is realized through the following steps:
[0026] 1) Weigh the reactants in the components according to the volume content, add 1 / 2 emulsifier and 1 / 2 initiator into 1 / 2 ion water, and form emulsified aqueous solution system A in the colloid mill;
[0027] 2) Mix acrylate and acrylic acid monomers according to the volume ratio, slowly add to the above emulsifier system A in the colloid mill, and emulsify for 40 minutes to form prepolymer emulsion B;
[0028] 3) Put the remaining emulsifier, initiator, ionized water and 1 / 4 of the prepolymer emulsion B into a three-necked flask with a stirrer and a condenser, and heat it to 80-85°C in a water bath;
[0029] 4) Drop the remaining prepolymer emulsion B into the flask within 2-3 hours, continue to react for 2-3 hours after the dropwise addition, cool down and discharge to obtain a homogeneous emulsified dispersion, which is the waterproof coating agent....
Embodiment 1
[0034] To prepare a waterproof outdoor rescue rope with a diameter of 9.5 mm, the water absorption rate after finishing is required to be within 5%.
[0035] step 1:
[0036] 1) Weigh 10 parts of acrylate by volume as a mixture of ethyl methacrylate and butyl acrylate, 10 parts of fluorine-containing acrylic acid monomer as dodecafluoroheptyl acrylate, 0.3 parts of ammonium persulfate as the initiator, and 0.3 parts of ammonium persulfate as the emulsifier Add 8 parts of O-15 and ethylene glycol butyl ether mixture, and 57 parts of deionized water;
[0037] 2) Add 1 / 2 emulsifier and 1 / 2 initiator to 1 / 2 ionized water to form emulsified aqueous solution system A in the colloid mill;
[0038] 3) Mix ethyl methacrylate, butyl acrylate mixture and dodecafluoroheptyl acrylate in proportion, slowly add to the above emulsifier system A in the colloid mill, and emulsify for 40 minutes to form prepolymer emulsion B;
[0039] 4) Put the remaining emulsifier, initiator, deionized water...
Embodiment 2
[0044] To prepare a mountaineering rope with a diameter of 10.5mm, the water absorption performance after finishing is required to be within 3%.
[0045] step 1:
[0046] 1) Weigh 20 parts of acrylate by volume as lauryl acrylate, 30 parts of fluorine-containing acrylic acid monomer as perfluoroalkylsulfonamidoethyl acrylate, 0.1 part of sodium persulfate as initiator, and perfluoroalkyl as emulsifier 10 parts of ethoxy ether alcohol, 30 parts of deionized water;
[0047] 2) Add 1 / 2 emulsifier and 1 / 2 initiator to 1 / 2 ionized water to form emulsified aqueous solution system A in the colloid mill;
[0048] 3) Mix lauryl acrylate and perfluoroalkylsulfonamidoethyl acrylate in proportion, slowly add to the above emulsifier system A in the colloid mill, and emulsify for 40 minutes to form prepolymer emulsion B;
[0049] 4) Put the remaining emulsifier, initiator, deionized water and 1 / 4 of the prepolymer emulsion B into a three-necked flask with a stirrer and a condenser, and he...
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