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Atomizing preparation method of TiAl powder

A vacuum smelting and crucible technology, applied in the field of atomization preparation of TiAl powder, can solve the problem of uneven particle size distribution of powder, and achieve the effect of good atomization effect, avoiding freezing and high efficiency

Active Publication Date: 2017-08-01
YANGZHOU FEILING ALLOY TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Part of the more advanced technology uses the centrifugal method to atomize the melt after being thrown out. In the process of using centrifugal throwing, the inventor has found through research that the blowing speed and angle of the gas in the atomization process after the melt is thrown out, the liquid The direction of the flow has an impact on the effect of atomization and the particle size of the powder after atomization, but the current centrifugal process adopts the method of blowing air after continuous centrifugation, which makes the particle size distribution of the prepared powder uneven

Method used

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Experimental program
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Embodiment Construction

[0011] The present invention will be further described below in conjunction with specific embodiments.

[0012] A method for preparing TiAl powder by atomization. Firstly, the alloy ingot with the required composition obtained by vacuum melting and pouring is placed in a crucible of a vacuum induction melting furnace, and then vacuumed to 10 -5 After pa, turn on the power supply of the vacuum induction heating coil and the heating power is 20KW. First, preheat the crucible with a lower power. When the temperature of the crucible reaches about 1200℃ as measured by the thermocouple, keep it for 5min, and then increase the heating power to 30KW. The ingot in the crucible is quickly heated, and the ingot is completely melted after about 15 minutes. The temperature of the alloy melt is measured by infrared temperature measuring equipment. After the melt is kept at 1730-1770°C for 2-3 minutes, the temperature of the melt is then increased After the superheat reaches 250-300℃, the melt i...

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PUM

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Abstract

The invention discloses an atomizing preparation method of TiAl powder. The method comprises the steps that vacuumizing and heating melting are conducted, and then a melt is introduced into a centrifugal nozzle; the centrifugal nozzle starts to centrifugally rotate, and argon is ejected through an inert gas nozzle simultaneously; meanwhile, a control system controls a solenoid valve at a liquid drainage port in the centrifugal nozzle to be switched on and switched off in a pulse manner, so that the melt is thrown away in a pulse manner, and a liquid flow ejected each time is rightly opposite to the ejection direction of atomized gas; frontal impact of the melt and the atomized gas is achieved, the melt is crushed into minute droplets under the action of airflow, and the minute droplets are cooled and solidified into fine powder; and the fine powder enters a collecting chamber, and then the fine powder is collected after being separated through a cyclone separator and sieved through a vibrating screen.

Description

Technical field [0001] The invention belongs to the technical field of material processing, and particularly relates to an atomized preparation method of TiAl powder. Background technique [0002] Titanium alloy has low density, high strength, high hardness, high temperature resistance, high corrosion resistance and friction resistance, especially TiAl intermetallic compound because of its high specific strength, high specific stiffness, corrosion resistance, wear resistance and high temperature resistance As well as the advantages of excellent oxidation resistance, it is becoming one of the excellent candidate structural materials in the contemporary aerospace industry, civil industry and other fields, especially in the field of aero engine blades. It has broad application prospects. 3D printing, or additive manufacturing, is a rapid prototyping process that has emerged in recent years. It adopts layer-by-layer powder spreading, laser or electron beam melting molding, to achieve...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F9/10
CPCB22F9/10
Inventor 王茜潘龙白嘉瑜
Owner YANGZHOU FEILING ALLOY TECH CO LTD
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