Preparation method of sludge-based charcoal slow-release phosphate fertilizer and sludge-based charcoal slow-release phosphate fertilizer
A technology of biochar and sludge, which is applied in the direction of phosphate fertilizer, ammonium orthophosphate fertilizer, pyrolysis treatment sludge, etc., can solve the problems of multi-energy and economic cost, high energy consumption of slow-release fertilizer, difficult process control, etc., and achieve shortening The effect of high treatment cycle, high treatment efficiency and high solid yield
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
preparation example Construction
[0023] The preparation method of the sludge-based biochar slow-release phosphate fertilizer of the embodiment of the present invention comprises the following steps:
[0024] S1: Add a conditioner to the sludge and stir evenly to obtain conditioned sludge.
[0025] Specifically, in the embodiment of the present invention, the water content of the sludge is 50-85wt%, and the added weight of the conditioner is 0.5%-10% of the dry solid weight of the sludge. The conditioner is steel slag waste, KOH, CaO, CaCO 3 、Al 2 o 3 , ZnCl 2 A mixture of one or more of inorganic conditioners. In the embodiment of the present invention, adding a conditioner to the sludge for conditioning can increase the porosity of the sludge, thereby making the reaction of the sludge in the subsequent steps more sufficient, thereby obtaining a higher yield of sludge-based biochar.
[0026] S2: Put the conditioned sludge into a hydrothermal reactor, seal it, and heat it for hydrothermal carbonization re...
Embodiment 1
[0041] S1: Add steel slag to the domestic sludge with a water content of 85wt%. The amount of steel slag added is 5.0% of the dry solid weight of the sludge. Stir evenly to obtain conditioned sludge.
[0042] S2: Put the conditioned sludge into a hydrothermal reactor, seal it, and microwave-assisted heating for hydrothermal carbonization reaction, wherein the microwave power is 400W, the reaction temperature is controlled at 200°C, the reaction time is 90min, and the hydrothermal carbonization reaction is carried out. The pressure inside the reactor is 2.4Mpa, and a hydrothermal carbonization liquid is obtained.
[0043] S3: The hydrothermal carbonization liquid is centrifuged at 3500 r / min for solid-liquid separation, and the separated solid product is washed three times with water, and dried in an oven at 50° C. to obtain sludge-based biochar.
[0044] S4: Place the sludge-based biochar in a potassium dihydrogen phosphate solution with a concentration of 200ppm, the solid-to...
Embodiment 2
[0047] S1: Dosing Al mixed in a 1:1 weight ratio to domestic sludge with a moisture content of 85wt% 2 o 3 and ZnCl 2 The mixed conditioner, the dosage of the mixed conditioner is 7.5% of the dry solid weight of the sludge, and the mixed conditioner is evenly stirred to obtain the conditioned sludge.
[0048] S2: Put the conditioned sludge into the hydrothermal reactor, seal it, and feed N 2 , wherein the reaction temperature is controlled at 250°C, the reaction time is 150min, and the pressure inside the hydrothermal reactor is about 5.0Mpa to obtain the hydrothermal carbonization liquid.
[0049] S3: The hydrothermal carbonization liquid is centrifuged at 3500 r / min for solid-liquid separation, and the separated solid product is washed three times with water, and dried in an oven at 50° C. to obtain sludge-based biochar.
[0050] S4: Place the sludge-based biochar in a diammonium phosphate solution with a concentration of 500ppm, the solid-to-liquid ratio of the sludge-ba...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com