Low-smoke halogen-free flame-retardant sealing strip and method for preparing same
A technology of sealing strips and intumescent flame retardants, which is applied in chemical instruments and methods, and other chemical processes, can solve the problems of insufficient flame retardancy, achieve good flame retardancy, reduce usage, and comprehensive performance Improved effect
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Embodiment 1
[0021] Embodiment 1 Preparation of intumescent flame retardant polyphosphate polyethyleneimine salt
[0022] Dissolve 10 kg of polyethyleneimine in 100 kg of methanol, add dropwise 20 kg of polyphosphoric acid aqueous solution with a mass concentration of 5%, react at 60°C for 1 hour, filter to obtain a precipitate, wash 3 times with methanol, Dry at ℃ for 12 hours to prepare intumescent flame retardant polyphosphate polyethyleneimine salt.
Embodiment 2
[0024] The preparation operation of the intumescent flame retardant poly(ethyleneimine polyphosphate) is the same as in Example 1. The feed ratio of polyethyleneimine to polyphosphoric acid is 100:50, the mass ratio of polyethyleneimine to methanol is 1:20, the mass concentration of polyphosphoric acid aqueous solution is 30%, the reaction temperature is 30°C, and the reaction time is 3 hours.
Embodiment 3
[0026] The preparation operation of the intumescent flame retardant poly(ethyleneimine polyphosphate) is the same as in Example 1. The feed ratio of polyethyleneimine to polyphosphoric acid is 100:20, the mass ratio of polyethyleneimine to methanol is 1:12, the mass concentration of polyphosphoric acid aqueous solution is 20%, the reaction temperature is 45°C, and the reaction time is 2 hours.
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