Preparation method of NiAl/WC composite with high-temperature wear resistance

A composite material, tungsten carbide technology, applied in the field of material science, can solve the problems of complex steps, poor uniformity of binder phase distribution, and pores in composite materials, and achieves the effect of simple process, excellent high temperature wear resistance, and reduced energy consumption.

Inactive Publication Date: 2017-09-08
SHANDONG UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] However, the sintering reaction method requires the raw materials to undergo a compound reaction, which seriously affects the shrinkage and density of the alloy, and will generate holes in the composite material;
[0007] The intermetallic compound pre-alloying method is to prepare NiAl intermetallic compound pre-alloy powder first, and the aggregate structure will be formed when preparing the intermetallic compound pre-alloy powder, resulting in poor uniformity of binder phase distribution and low compositional stability. It needs to go through two sintering steps, the steps are complicated, the material preparation time is long, and the energy consumption is high

Method used

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  • Preparation method of NiAl/WC composite with high-temperature wear resistance
  • Preparation method of NiAl/WC composite with high-temperature wear resistance
  • Preparation method of NiAl/WC composite with high-temperature wear resistance

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] Embodiment 1 A kind of preparation method of nickel-aluminum-tungsten carbide composite material resistant to high temperature wear

[0035] (1) Ingredients

[0036] The specifications among the raw materials used in this process are as follows:

[0037] Ni powder: particle size is 200 mesh, purity 99.0%;

[0038] Al powder: particle size is 200 mesh, purity 99.5%;

[0039] WC powder: particle size is 200 mesh, purity 99.5%.

[0040] Mix Ni powder and Al powder according to the molar ratio of 1:1, then mix the Ni-Al mixed powder with WC powder, mill the mixed powder in a planetary ball mill for 2 hours, and the speed of ball milling is 300r / min to obtain a uniform mixture Ni-Al-WC mixed powder;

[0041] The mass percentage of WC powder in Ni-Al-WC mixed powder is 5%.

[0042] Compact

[0043] Apply a pressure of 200MPa to the Ni-Al-WC mixed powder mixed in step (1) to press into a compact; the compact is pressed into a cylindrical blank with a diameter of 40mm×30m...

Embodiment 2

[0046]Embodiment 2 A kind of preparation method of nickel-aluminum-tungsten carbide composite material resistant to high temperature wear

[0047] (1) Ingredients

[0048] The specifications among the raw materials used in this process are as follows:

[0049] Ni powder: particle size is 200 mesh, purity 99.0%;

[0050] Al powder: particle size is 200 mesh, purity 99.5%;

[0051] WC powder: particle size is 100 mesh, purity 99.5%.

[0052] Mix Ni powder and Al powder according to the molar ratio of 1:1, then mix the Ni-Al mixed powder with WC powder, mill the mixed powder in a planetary ball mill for 2 hours, and the speed of ball milling is 300r / min to obtain a uniform mixture Ni-Al-WC mixed powder;

[0053] The mass percentage of WC powder in the Ni-Al-WC mixed powder is 30%.

[0054] Compact

[0055] The Ni-Al-WC mixed powder mixed in step (1) is pressed into a compact under a pressure of 200MPa; the compact is pressed into a cylindrical blank with a diameter of 40mm×...

Embodiment 3

[0058] Embodiment 3 A kind of preparation method of nickel-aluminum-tungsten carbide composite material resistant to high temperature wear

[0059] (1) Ingredients

[0060] The specifications among the raw materials used in this process are as follows:

[0061] Ni powder: the particle size is 100 mesh, the purity is 95%;

[0062] Al powder: particle size is 100 mesh, purity 95%;

[0063] WC powder: the particle size is 100 mesh, and the purity is 95%.

[0064] Mix Ni powder and Al powder according to the molar ratio of 1:1, then mix the Ni-Al mixed powder with WC powder, mill the mixed powder in a planetary ball mill for 2 hours, and the speed of ball milling is 300r / min to obtain a uniform mixture Ni-Al-WC mixed powder;

[0065] The mass percentage of WC powder in the Ni-Al-WC mixed powder is 10%.

[0066] Compact

[0067] Apply a pressure of 350MPa to the Ni-Al-WC mixed powder mixed in step (1) to press into a compact; the compact is pressed into a cylindrical blank wi...

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Abstract

The invention provides a NiAl/WC composite with the high-temperature wear resistance and a preparation method of the composite. The composite is prepared from raw materials including Ni powder, Al powder and WC powder; the mole ratio of the Ni powder to the Al powder is 1:1; the mass of the WC powder accounts for 5wt%-40wt% of the total mass of Ni-Al-WC mixed powder; the Ni powder has the particle size ranging from 100 meshes to 300 meshes and the purity ranging from 95%-99.5%; the Al powder has the particle size ranging from 100 meshes to 300 meshes and the purity ranging from 95%-99.5%; and the WC powder has the particle size ranging from 100 meshes to 300 meshes and the purity ranging from 95%-99.5%. With the preparation method, high-temperature sintering is not required, so that the obtained composite is uniform in structure, free of pores and high in stability.

Description

technical field [0001] The invention belongs to the field of material science and technology, and mainly relates to a method for preparing a nickel-aluminum-tungsten carbide (NiAl / WC) composite material by adopting a thermal explosion synthesis auxiliary pressurization process. Background technique [0002] Nickel-aluminum (NiAl) intermetallic compounds have excellent high-temperature comprehensive performance, high melting point and low density, and can be widely used in aerospace and electric boiler fields that require high-temperature performance of materials. However, NiAl intermetallic compounds have poor high-temperature wear resistance and cannot be used under high-temperature and large-load contact friction conditions. [0003] At present, the application of nickel-aluminum-tungsten carbide (NiAl / WC) composite materials in China is mainly concentrated in cemented carbide, which is prepared by thermal explosion synthesis or high-temperature sintering. The research an...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C19/03C22C32/00C22C1/05
CPCC22C1/058C22C19/007C22C19/03C22C32/0052
Inventor 袁建军刘欣颖娄淑梅李东民
Owner SHANDONG UNIV OF SCI & TECH
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