Multilayer hollow composite wave-absorbing material
A composite wave-absorbing material and hollow structure technology, applied in the field of wave-absorbing materials, can solve problems such as poor absorption of low-frequency microwaves and high density of ferrite, and achieve increased dielectric constant, increased magnetic permeability, and increased absorbing loss. Effect
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Embodiment 1
[0045] Step 1, prepare hollow nickel
[0046] a) carbonyl iron powder pretreatment
[0047] Ultrasonically treat carbonyl iron powder with a particle size of about 5 μm in acetone for 50 minutes to remove impurities on its surface, then soak it in 1mol / L dilute hydrochloric acid for 20 seconds to remove the oxide film on its surface, and put it away after treatment Dry in a vacuum oven;
[0048] b) Configure the plating solution
[0049] Mix 0.1mol / L nickel sulfate solution and 40g / L sodium tartrate solution, after fully stirring, add 0.8g / L thiourea solution and continue stirring to allow thiourea to fully dissolve, then add 55g / L hydrazine hydrate solution, fully Stir evenly to obtain a turbid solution, add 1mol / L sodium hydroxide solution to the turbid solution to adjust the pH to 11 while stirring, so that the turbid solution becomes a solution without precipitation, which is the nickel plating solution;
[0050] c) Nickel plating
[0051] Put the prepared plating solu...
Embodiment 2
[0065] Step 1, prepare hollow nickel
[0066] a) carbonyl iron powder pretreatment
[0067] Ultrasonically treat carbonyl iron powder with a particle size of about 5 μm in acetone for 50 minutes to remove impurities on its surface, then soak it in 1mol / L dilute hydrochloric acid for 20 seconds to remove the oxide film on its surface, and put it away after treatment Dry in a vacuum oven;
[0068] b) Configure the plating solution
[0069] Mix 0.1mol / L nickel sulfate solution and 40g / L sodium tartrate solution, after fully stirring, add 0.8g / L thiourea solution and continue stirring to allow thiourea to fully dissolve, then add 55g / L hydrazine hydrate solution, fully Stir evenly to obtain a turbid solution, add 1mol / L sodium hydroxide solution to the turbid solution to adjust the pH to 11 while stirring, so that the turbid solution becomes a solution without precipitation, which is the nickel plating solution;
[0070] c) Nickel plating
[0071] Put the prepared plating solu...
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