A kind of preparation method of high-performance gesbte-based thermoelectric material
A technology of thermoelectric materials and raw materials, which is applied in the manufacture/processing of thermoelectric devices, and lead-out wire materials of thermoelectric devices. , the effect of reducing the carrier concentration and improving the thermoelectric performance
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Embodiment 1
[0034] A method for preparing a high-performance GeSbTe-based thermoelectric material, comprising the steps of:
[0035] 1) Using Ge, Sb and Te simple substances as raw materials, according to Ge 0.93 Sb 0.06 The stoichiometric ratio of Te weighs each raw material, puts the weighed raw material into a quartz test tube and vacuum seals it, then puts the quartz tube into a melting furnace and heats it to 1100°C for 24 hours until the reaction is complete, and finally cools to room temperature with the furnace. Ingot product;
[0036] 2) Place the ingot product obtained in step 1) in a quartz tube with a nozzle diameter of 0.5mm, place the quartz tube above the radio frequency copper roller for induction melting, and spray the molten alloy obtained by smelting on a 10m On the copper roller that rotates at / s, the thin strip product is obtained;
[0037] 3) Grind the strip product obtained in step 2), and then perform PAS sintering at a temperature of 500°C and a pressure of 50...
Embodiment 2
[0040] A method for preparing a high-performance GeSbTe-based thermoelectric material, comprising the steps of:
[0041] 1) Using Ge, Sb and Te simple substances as raw materials, according to Ge 0.98 Sb 0.01The stoichiometric ratio of Te weighs each raw material, puts the weighed raw material into a quartz test tube and vacuum seals it, then puts the quartz tube into a melting furnace and heats it to 1100°C for 24 hours until the reaction is complete, and finally cools to room temperature with the furnace. Ingot product;
[0042] 2) Place the ingot product obtained in step 1) in a quartz tube with a nozzle of 0.5mm in diameter, and place the quartz tube above the radio frequency copper roller for induction melting. On the copper roller that rotates at / s, a thin strip product is obtained;
[0043] 3) Grinding the ribbon product obtained in step 2), and then performing PAS sintering at a temperature of 480° C. and a pressure of 52 MPa for 5 minutes to obtain a dense block, ...
Embodiment 3
[0045] A method for preparing a high-performance GeSbTe-based thermoelectric material, comprising the steps of:
[0046] 1) Using Ge, Sb and Te simple substances as raw materials, according to Ge 0.89 Sb 0.1 The stoichiometric ratio of Te weighs each raw material, puts the weighed raw material into a quartz test tube and vacuum seals it, then puts the quartz tube into a melting furnace and heats it to 1100°C for 24 hours until the reaction is complete, and finally cools to room temperature with the furnace. Ingot product;
[0047] 2) Place the ingot product obtained in step 1) in a quartz tube with a nozzle diameter of 0.5mm, place the quartz tube above the radio frequency copper roller for induction melting, and spray the molten alloy obtained by smelting on a 10m On the copper roller that rotates at / s, a thin strip product is obtained;
[0048] 3) Grinding the ribbon product obtained in step 2), and then performing PAS sintering at a temperature of 520° C. and a pressure...
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