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Magnetic wool fabric prepared by using inorganic sulfur-containing reductive agent

A technology of reducing agent and wool, which is applied in the field of using inorganic sulfur-containing reducing agent to prepare magnetic wool fabric, which can solve the problems of difficult control, long process, low washing fastness, etc., and achieve the effect of reducing damage

Inactive Publication Date: 2017-11-24
SOUTHWEST UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the adsorption method mainly uses the intermolecular van der Waals force and ionic bond force to make the nanoparticles adsorb to the surface of the wool fiber, and the washing fastness is low; the process of the sol-gel method and the layer-by-layer assembly method is long and difficult to control; The coating method is to use adhesives to bond nanoparticles to the surface of wool fibers, which reduces the skin affinity of wool fibers to the human body

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] (1) Dissolve 3.5g of sodium sulfide, 40g of urea and 3g of sodium lauryl sulfate into water to form a 100g mixed solution, then add 0.3g of magnetic nano-particle nickel ferrite, and stir vigorously to prepare a dispersed magnetic nano-particle nickel Ferrite solution;

[0014] (2) padding the woolen fabric in the solution solution obtained in step (1) several times, and the excess rate is 80%;

[0015] (3) Heat the padded wool fabric under hot air at 120°C for 15 minutes;

[0016] (4) Soak the heated wool fabric in saturated sodium chloride aqueous solution for 10 minutes, then wash and dry.

Embodiment 2

[0018] (1) Dissolve 4g of sodium metabisulfite, 30g of urea and 4g of sodium lauryl sulfate into water to form a 100g mixed solution, then add 0.8g of magnetic nanoparticle cobalt ferrite, and stir vigorously to prepare cobalt iron with magnetic nanoparticles dispersed Oxygen solution;

[0019] (2) padding the woolen fabric in the solution solution obtained in step (1) several times, and the excess rate is 100%;

[0020] (3) Heat the padded wool fabric under hot air at 120°C for 15 minutes;

[0021] (4) Soak the heated wool fabric in saturated sodium chloride aqueous solution for 10 minutes, then wash and dry.

Embodiment 3

[0023] (1) Dissolve 5g of sodium bisulfite, 50g of urea and 2g of sodium lauryl sulfate into water to form a 100g mixed solution, then add 1.2g of magnetic nanoparticle magnesium ferrite, and stir vigorously to prepare dispersed magnetic nanoparticles Dissolving solution of magnesium ferrite;

[0024] (2) padding the woolen fabric in the solution solution obtained in step (1) several times, and the excess rate is 90%;

[0025] (3) Heat the padded wool fabric under hot air at 80°C for 30 minutes;

[0026] (4) Soak the heated wool fabric in saturated sodium chloride aqueous solution for 10 minutes, then wash and dry.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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PUM

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Abstract

The present invention provides a method for preparing magnetic wool fabrics using an inorganic sulfur-containing reducing agent, the method comprising the following steps: (1) Preparation of a solution: dissolving the inorganic sulfur-containing reducing agent, urea and sodium lauryl sulfate into water, then add magnetic nanoparticles, stir vigorously to prepare a solution in which magnetic nanoparticles are dispersed; (2) pad the wool fabric in the solution obtained in step (1) for several times; (3) pad the The woolen fabric is heated under hot air; (4) The heated woolen fabric is soaked in saturated sodium chloride aqueous solution to solidify, then washed and dried. The preparation technology is simple and easy, the cost is low, the strength damage to the wool fabric is small, the surface properties of the wool fiber are not changed, and the magnetic nanoparticles have good fastness on the wool fabric; no adhesive is used in the preparation process, and no Poison is harmless.

Description

technical field [0001] The invention relates to a method for preparing functional fabrics, in particular to a method for preparing magnetic wool fabrics by using an inorganic sulfur-containing reducing agent. Background technique [0002] Functional fiber materials can be prepared by introducing nanoparticles into textile fibers. At present, there are many preparation methods for introducing nanoparticles into wool fibers, such as: adsorption method, sol-gel method, layer-by-layer assembly method, coating method and so on. However, the adsorption method mainly uses the intermolecular van der Waals force and ionic bond force to make the nanoparticles adsorb to the surface of the wool fiber, and the washing fastness is low; the process of the sol-gel method and the layer-by-layer assembly method is long and difficult to control; The coating method is to use adhesives to bond nanoparticles to the surface of wool fibers, which reduces the skin affinity of wool fibers to the hum...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M11/49D06M11/53D06M11/54D06M11/51D06M13/262D06M13/432D06M11/13D06M10/06D06M10/08D06M101/12
CPCD06M11/49D06M10/06D06M10/08D06M11/13D06M11/51D06M11/53D06M11/54D06M13/262D06M13/432D06M2101/12
Inventor 卢明刘一萍
Owner SOUTHWEST UNIVERSITY
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