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Method for preparing high-performance lubricating oil additive by deeply processing petroleum heavy oil

A lubricating oil additive, petroleum heavy oil technology, applied in the direction of additives, petroleum industry, lubricating composition, etc., can solve the problems of graphite dispersion, cracking or even collapse, graphite surface structure change, corrosion of mechanical metal objects and oil seals, etc., to achieve reduction Excellent friction and anti-wear effect, good dispersion and stability, and simple preparation process

Active Publication Date: 2018-03-09
河北中圣博泰科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the problem is that when graphite is used in an oxygen-containing environment higher than 325 °C, the boundary carbon atoms are easy to react with oxygen and oxidize to form carbon dioxide, so that the surface structure of graphite changes and loses its lubricating effect. Dispersion, cracking or even collapse at the edge will reduce the timeliness of graphite use; both molybdenum disulfide and tungsten disulfide are easy to react with oxygen at high temperature to form sulfur, so when sulfur reacts with water vapor to produce sulfuric acid, It may corrode the metal objects and oil seals in the machine, and cause damage to the machine
But it has not announced the preparation method of the nano-carbon spheres, let alone the method for preparing the nano-carbon spheres from petroleum heavy oil

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Embodiment 1, the preparation method of a kind of deep processing of petroleum heavy oil mentioned in the present invention prepares high-performance lubricating oil additive, its specific steps are as follows:

[0024] The petroleum heavy oil is introduced into the filter from the storage tank for deashing and slag removal, and then enters the dehydration tower to remove the water content of the raw material to below 0.5%, and the processed petroleum heavy oil is added to the petroleum heavy oil as needed. Elemental metal Fe, adding 0.2% (mass ratio) into the petroleum heavy oil storage tank, pump the petroleum heavy oil into the thermal polymerization circulation pipe, use a vacuum pump to evacuate the thermal polymerization circulation pipe, turn on the thermal polymerization circulation pipe circulation pump, Petroleum heavy oil circulates in the thermal polymerization circulation pipe, and the thermal polymerization heating furnace is used to heat the circulation pi...

Embodiment 2

[0029] Embodiment 2, the preparation method of a kind of deep processing of petroleum heavy oil mentioned in the present invention prepares high-performance lubricating oil additive, its specific steps are as follows:

[0030] The petroleum heavy oil is introduced from the storage tank into the filter for deashing and slag removal, and then enters the dehydration tower to remove the water content of the raw material to below 0.5%, and the processed petroleum heavy oil (can also be added to the heavy oil as needed Nano-metal elemental Cu, add 0.2% (mass ratio) into the petroleum heavy oil storage tank, pump the petroleum heavy oil into the thermal polymerization circulation pipe, use a vacuum pump to vacuum the thermal polymerization circulation pipe, turn on the thermal polymerization circulation pipe circulation pump , petroleum heavy oil circulates in the thermal polymerization circulation pipe, and the thermal polymerization heating furnace is used to heat the circulation pi...

Embodiment 3

[0033] Embodiment 3, the preparation method of a kind of deep processing of petroleum heavy oil mentioned in the present invention prepares high-performance lubricating oil additive, its specific steps are as follows:

[0034] The petroleum heavy oil is introduced from the storage tank into the filter for deashing and slag removal, and then enters the dehydration tower to remove the water content of the raw material to below 0.5%, and the processed petroleum heavy oil (can also be added to the heavy oil as needed Nano-metal elemental Ni, adding 0.4% (mass ratio) into the petroleum heavy oil storage tank, pump the petroleum heavy oil into the thermal polymerization circulation pipe, use a vacuum pump to evacuate the thermal polymerization circulation pipe, and turn on the thermal polymerization circulation pipe circulation pump , The petroleum heavy oil circulates in the thermal polymerization circulation pipe, and the thermal polymerization heating furnace is used to heat the c...

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Abstract

The invention relates to a method for preparing a high-performance lubricating oil additive by deeply processing petroleum heavy oil. According to the technical scheme, the method comprises the following steps: 1) adding metal elements to petroleum heavy oil in order to increase the forming speed of nano carbon liquid crystal balls; 2) charging heavy oil into a thermal polymerizing circulating pipe through a pump; vacuumizing; and forming nano carbon liquid crystal balls in the petroleum heavy oil by the thermal polymerizing reaction; 3) removing impurities such as No, O and S in the heavy oilby hydrofining cracking; splitting some light components, intermediate components and heavy components, wherein most of the nano carbon liquid crystal balls are dissolved in the intermediate components; and 4) treating the oily liquid as the high-performance lubricating oil additive. The method has the beneficial effects that the intermediate components subjected to hydrofining cracking are treated by removing the impurities such as N, O and S in the heavy oil, and then the oily liquid is treated as the high-performance lubricating oil additive; the method is simple in preparation processes,energy saving, environmentally friendly, and easy to popularize; and a new way is provided for development and utilization of the petroleum heavy oil.

Description

technical field [0001] The invention relates to a lubricating oil additive, in particular to a method for preparing a high-performance lubricating oil additive through deep processing of petroleum heavy oil. Background technique [0002] Lubricating oil is widely used in the national economy, especially in the machinery industry. In the 21st century, many working conditions have exceeded the use limit of conventional lubricating oils, and there is an urgent need for high-temperature lubricating oils to meet the harsh operating environments. In order to improve the performance of lubricating oil, solid lubricating additives are often added to lubricating oil, generally including graphite, molybdenum disulfide, tungsten disulfide and polytetrafluoroethylene. However, the problem is that when graphite is used in an oxygen-containing environment higher than 325 °C, the boundary carbon atoms are easy to react with oxygen and oxidize to form carbon dioxide, so that the surface st...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M159/04B82Y40/00C10G69/12C10N50/08C10N30/06C10N30/04
CPCC10M141/00C10M2201/041C10M2203/10
Inventor 李明熊珂英张子鹏李波张兆杰
Owner 河北中圣博泰科技有限公司
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