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Production technique of high-performance permanent magnetic ferrite pre-sintered material

A permanent magnet ferrite and production process technology, which is applied in the production process field of pre-sintered materials, can solve the problems of increased production cost, production waste, and sintered products with different sizes, so as to improve the overall strength, reduce the production cycle, The effect of reducing production waste

Inactive Publication Date: 2018-04-24
HUNAN AEROSPACE MAGNET & MAGNETO
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The following problems exist in the purchased calcined materials: the raw material shrinkage is unstable, and molding molds with different proportions need to be configured, and the mold manufacturing cost is quite high; the raw material shrinkage is unstable, which leads to different sizes of sintered products, resulting in less grinding during the grinding process. Or too much grinding, which affects the customer's index requirements, and at the same time produces a large amount of production waste, reduces the pass rate of the entire industrial chain, and increases production costs.

Method used

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  • Production technique of high-performance permanent magnetic ferrite pre-sintered material
  • Production technique of high-performance permanent magnetic ferrite pre-sintered material

Examples

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Effect test

Embodiment 1

[0020] A production process of high-performance permanent ferrite pre-fired material, the specific steps include: placing the mixture of ferrite red iron and strontium carbonate in a mixing tower, adding water, grinding, and passing through an X-ray fluorescence analyzer Carry out iron red and strontium carbonate composition correction, the mass percentage of iron red and strontium carbonate is 6.4; the composition corrected mixture is transported to the centrifugal dehydrator mixing tower for dehydration; then the high-concentration slurry is transported to the rotary kiln for pre-burning and cooling The kiln is cooled, and finally enters the ball mill for pulverization, and is ready; in the centrifugal dehydration stage, the water content of the mixed slurry is controlled at 35%; in the pre-sintering stage, the sintering feed rate is controlled at 1.5T / h, and the feed end The temperature of the kiln box is controlled at 330℃, and the high temperature sintering temperature of t...

Embodiment 2

[0022] A production process of high-performance permanent ferrite pre-fired material, the specific steps include: placing the mixture of ferrite red iron and strontium carbonate in a mixing tower, adding water, grinding, and passing through an X-ray fluorescence analyzer Carry out iron red and strontium carbonate composition correction, the mass percentage of iron red and strontium carbonate is 6.6; the composition-corrected mixture is transported to the centrifugal dehydrator mixing tower for dehydration; then the high-concentration slurry is transported to the rotary kiln for pre-burning and cooling The kiln is cooled, and finally enters the ball mill for pulverization, which is finished; in the centrifugal dehydration stage, the water content of the mixed slurry is controlled at 40%; in the pre-sintering stage, the sintering feed rate is controlled at 2.0T / h, and the feed end The temperature of the kiln box is controlled at 340℃, and the high temperature sintering temperature...

Embodiment 3~5

[0025] In Examples 3 to 5, 500g of permanent ferrite pre-fired material, 8.5 calcium carbonate, 3g boric acid, 3g alumina and 1.5g ammonium bicarbonate were placed in a ball mill, 1000g of water was added, and the ball milled to an average particle size of 0.8μm. Slurry, the ball milled slurry is filtered and precipitated to a water content of 33wt%; the filtered and precipitated slurry is injected into the mold, and the magnetic field strength is 530kA / m, the pressure is 15Mpa, and the pressure is 65s to form a diameter of Φ30 .1mm round cake shaped green body; put the formed green body into a sintering electric kiln at a heating rate of 3°C / min, at 1170~1190°C (see Table 1 for the temperature of each embodiment), sinter for 120min, The upper and lower surfaces of the sintered round cake are ground and polished to obtain permanent ferrite.

[0026] The TYU-2000 type magnetic material automatic measuring device is used to test the magnetic properties of the products. The test res...

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Abstract

The invention discloses a production technique of a high-performance permanent magnetic ferrite pre-sintered material. The technique comprises steps as follows: a mixture of iron oxide red and strontium carbonate as raw materials of permanent magnetic ferrite is put in a mixing tower, water is added, grinding is performed, composition correction of iron oxide red and strontium carbonate is executed by an X-ray fluorescence analyzer, and a ratio of iron oxide red to strontium carbonate is 5.95-6.55 in percentage by mass; a mixed material obtained after the composition correction is conveyed toa centrifugal dehydrator agitating tower for dehydrating; high-concentration slurry is conveyed to a rotary kiln for pre-sintering and conveyed to a cooling kiln for cooling, finally, a product entersa ball mill for smashing, and the pre-sintered material is obtained; water content of the mixed slurry is controlled in a range of 35%-45%; in the pre-sintering stage, the feed quantity of sinteringis controlled to be 1.5T-2.5T / h, and kiln temperature of the feeding end is controlled to be 320-360 DEG C; in the ball milling stage, the granularity of the finished product is controlled to be 3-8 mu m. According to the method, batch production of the high-performance permanent magnetic ferrite pre-sintered material is realized, bottleneck of outsourcing of the pre-sintered material for a long time is solved, and stability of follow-up industry chains of the company is guaranteed.

Description

Technical field [0001] The invention relates to a production process method of permanent ferrite calcination material, in particular to a production process method of high performance permanent ferrite body calcination material. Background technique [0002] With the rapid development of the market economy and the rapid social development, the competition among manufacturing industries has become increasingly fierce, and technological innovation and breakthroughs are imminent. However, the company's pre-fired ferrite formulations have long relied on external purchases, and the production costs are high. [0003] There are two methods for traditional pre-burned material production: 1. Dry preparation (1) raw material preparation; (2) dry ball milling; (3) pelletizing; (4) low temperature pre-burning: (5) pelletizing; (6) Pre-burning at high temperature; (7) Coarse crushing. 2. Wet preparation (1) Preparation of raw materials; (2) Chemical slurry of raw materials; (3) Grinding and m...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/26C04B35/626
CPCC04B35/26C04B35/62605
Inventor 王玉明郑亮邓兴民张春儒汪斌
Owner HUNAN AEROSPACE MAGNET & MAGNETO
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