An anti-sedimentation agent for ink used for marking and coding of steel pipes before leaving the factory
An anti-sedimentation agent and marking technology, applied in the field of steel pipe marking, to achieve excellent anti-settling performance, improve blending compatibility, and excellent water solubility
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Embodiment 1
[0020] (1) Preparation of hydrogenated castor oil intercalated zeolite powder: the natural zeolite is crushed by a jet mill and passed through a 100-mesh sieve, and calcined at 500-550° C. to constant weight, and naturally cooled to room temperature to obtain calcined zeolite powder; Add 20g of calcined zeolite powder and 5g of hydrogenated castor oil into 100g of water, and stir to form a slurry. The resulting slurry is treated with microwave reflux for 5 minutes using a microwave processor with a microwave frequency of 2450MHz and an output power of 700W. After stirring for 15 minutes, continue the microwave reflux treatment for 5 minutes, and stir After 15 minutes, microwave reflux treatment for 5 minutes again, and repeat until the viscosity of the obtained slurry does not change, and then send the obtained slurry into a spray dryer, and dry the obtained particles into a micropowder through an ultrafine pulverizer to obtain hydrogenated castor oil intercalation Zeolite powd...
Embodiment 2
[0024] (1) Preparation of hydrogenated castor oil intercalated zeolite powder: the natural zeolite is crushed by a jet mill and passed through a 100-mesh sieve, and calcined at 500-550° C. to constant weight, and naturally cooled to room temperature to obtain calcined zeolite powder; Add 25g of calcined zeolite powder and 8g of hydrogenated castor oil into 100g of water, stir to form a slurry, and use a microwave processor with a microwave frequency of 2450MHz and an output power of 700W to treat the resulting slurry under microwave reflux for 5 minutes. After stirring for 15 minutes, continue the microwave reflux treatment for 5 minutes. After 15 minutes, microwave reflux treatment for 5 minutes again, and repeat until the viscosity of the obtained slurry does not change, and then send the obtained slurry into a spray dryer, and dry the obtained particles into a micropowder through an ultrafine pulverizer to obtain hydrogenated castor oil intercalation Zeolite powder;
[0025...
Embodiment 3
[0039] The anti-sedimentation agents prepared in Examples 1-2 and Comparative Examples 1-3 were prepared into water-based steel pipe inkjet inks according to the ratio of raw materials shown in Table 1, and the performance of the prepared water-based steel pipe inkjet inks was measured, and the results As shown in table 2.
[0040] Table 1 Raw material ratio of water-based steel pipe inkjet ink
[0041] raw material Example 1 Example 2 Comparative example 1 Comparative example 2 Comparative example 3 Nano White Pigment 15g 15g 15g 15g 15g Waterborne Epoxy Emulsion 15g 15g 15g 15g 15g Polyethylene glycol 600 3g 3g 3g 3g 3g Anti-settling agent 2g 2g 2g 2g 2g Propylene glycol butyl ether 2g 2g 2g 2g 2g water 50g 50g 50g 50g 50g
[0042] Table 2 Performance of water-based steel pipe inkjet ink
[0043] group Abrasion / g Light fastness grade Pigment sedimentation rate after standing f...
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