Preparation method of flame-retardant cable material
A technology for flame-retardant cable materials and preparation steps, which is applied in the direction of plastic/resin/wax insulators, organic insulators, etc., which can solve the problems of poor carbonization ability and easy burning of cable material matrix resin, and achieve low crystallinity and good compatibility Effect
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[0025] Example 1
[0026] Mix 400 mL of sodium hydroxide solution with a mass fraction of 40% and 80 g of aluminum hydroxide, put it in a stainless steel pot, heat it up to 200 ° C through a resistance furnace, and cook for 20 min to obtain a cooking liquid. Filter the cooking liquid with a microporous membrane, Remove the solid residue to obtain a sodium aluminate solution; mix the aluminum sulfate solution with a mass fraction of 30% and the above-mentioned sodium aluminate solution in an equal volume ratio, add it to a beaker, heat the beaker in a water bath and raise the temperature to 70 ° C, stir for 10 min, and keep the temperature. React for 30min to obtain a reaction product, place the reaction product in a high-speed centrifuge at a rotational speed of 4500r / min for 15min, separate and remove the upper layer liquid to obtain a lower layer precipitate, wash the precipitate with water until the washing liquid is neutral, and obtain a supernatant. Refine aluminum hydrox...
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[0027] Example 2
[0028]Mix 450 mL of sodium hydroxide solution with a mass fraction of 40% and 85 g of aluminum hydroxide, put it in a stainless steel pot, heat it up to 215 ° C through a resistance furnace, and cook for 23 minutes to obtain a cooking liquid. Filter the cooking liquid with a microporous membrane, Remove the solid residue to obtain a sodium aluminate solution; mix the aluminum sulfate solution with a mass fraction of 30% and the above-mentioned sodium aluminate solution in an equal volume ratio, add it to a beaker, heat the beaker in a water bath and heat up to 73 ° C, stir for 13 min, and keep the temperature. React for 33min to obtain a reaction product, place the reaction product in a high-speed centrifuge at 4650r / min for centrifugation for 17min, separate and remove the upper layer liquid to obtain a lower layer precipitate, wash the precipitate with water until the washing liquid is neutral, and obtain a supernatant. Refining aluminum hydroxide; placing...
Example Embodiment
[0029] Example 3
[0030] Mix 500 mL of sodium hydroxide solution with a mass fraction of 40% and 90 g of aluminum hydroxide, put it in a stainless steel pot, heat it up to 230 ° C through a resistance furnace, and cook for 25 minutes to obtain a cooking liquid. Filter the cooking liquid with a microporous membrane, Remove the solid residue to obtain a sodium aluminate solution; mix the aluminum sulfate solution with a mass fraction of 30% and the above-mentioned sodium aluminate solution in an equal volume ratio, add it to a beaker, heat the beaker in a water bath and heat up to 75 ° C, stir for 15min, and keep the temperature. React for 35min to obtain a reaction product, place the reaction product in a high-speed centrifuge at 4800r / min for centrifugation for 20min, separate and remove the upper layer liquid to obtain a lower layer precipitate, wash the precipitate with water until the washing liquid is neutral, and obtain a supernatant. Refine aluminum hydroxide; put the u...
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