Preparation method of novel heat isolating nanometer material
A technology of nano-materials and nano-composites, which is applied in the field of preparation of new heat-insulating nano-composites, can solve the problems of poor high-temperature resistance of heat-insulating materials, limit the application of heat-insulating materials, and reduce the heat-insulation performance of heat-insulating materials, etc. Cross-linking degree, improvement of heat insulation effect, effect of lowering thermal conductivity
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Embodiment 1
[0016] A method for preparing a novel heat-insulating nanomaterial, the method comprising the following steps:
[0017] Step 1, 36 parts of Cu-BTC-SiO 2 Nanomaterials, 12 parts of polyethylene resin, 3 parts of polycarbonate, 6 parts of barium stearate and 5 parts of glass fiber are mixed and stirred in a mixer to form a mixed slurry;
[0018] Step 2. Transfer the above slurry to a reaction kettle, heat to 80°C under the protection of argon, add 8 parts of ethyl methacrylate and 3 parts of ethylene oxide, stir for 30 minutes, and then heat up to 75°C. Add 5 parts of alumina, continue to stir for 60 minutes, and obtain the green body material after drying;
[0019] Step 3. Neatly put the green body material prepared in the above steps into the mold, then put the mold into the molding press for one-time molding and pressing, and then perform pressure curing. The curing temperature is from room temperature to 175°C, and the curing time is 3 Hour;
[0020] Step 4. Put the solid...
Embodiment 2
[0027] Step 1, 26 parts of Cu-BTC-SiO 2 Nanomaterials, 22 parts of polyethylene resin, 3 parts of polycarbonate, 6 parts of barium stearate and 5 parts of glass fiber are mixed and stirred in a mixer to form a mixed slurry;
[0028] Step 2. Transfer the above slurry to a reaction kettle, heat to 80°C under the protection of argon, add 8 parts of ethyl methacrylate and 3 parts of ethylene oxide, stir for 30 minutes, and then heat up to 75°C. Add 5 parts of alumina, continue to stir for 60 minutes, and obtain the green body material after drying; the rest of the preparation is the same as in Example 1.
Embodiment 3
[0030] Step 1, 19 parts of Cu-BTC-SiO 2 Nanomaterials, 14 parts of polyethylene resin, 3 parts of polycarbonate, 6 parts of barium stearate and 5 parts of glass fiber are mixed and stirred in a mixer to form a mixed slurry;
[0031] Step 2. Transfer the above slurry to a reaction kettle, heat to 80°C under the protection of argon, add 8 parts of ethyl methacrylate and 3 parts of ethylene oxide, stir for 30 minutes, and then heat up to 75°C. Add 5 parts of alumina, continue to stir for 60 minutes, and obtain the green body material after drying; the rest of the preparation is the same as in Example 1.
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