Preparation method of tableware disinfectant
A disinfectant and tableware technology, applied in the direction of disinfectants, botany equipment and methods, chemical instruments and methods, etc., can solve problems such as human hazards, achieve low surface and interfacial tension, good detergency, and improve the effect of use
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[0022] A preparation method of a tableware disinfectant, the preparation method comprising the following steps:
[0023] (1) According to the mass ratio of 7~8: 2~3: 0.01~0.02, mix soluble starch, dodecanol, and catalyst, stir at 110~120℃, 200~300r / min for 1~2h, in vacuum Keep the temperature at 0.01~0.03MPa for 1~2h, adjust the pH value to 8~9, wait to cool to room temperature, filter to obtain the filter residue, according to the mass ratio of 1:3~4, mix the filter residue and hydrogen peroxide for 1~2h, filter , Get the decolorized product, wash the decolorized product with ethanol 2~3 times, and dry it at a temperature of 50~60℃ to obtain the dried product for use;
[0024] (2) Dry the citrus peel at a temperature of 60~70℃, pulverize, and pass through a 30-40 mesh sieve to obtain a sieved product. According to a mass ratio of 1:5-6, the sieved product and petroleum ether are mixed and degreased. Filter, separate the filtrate and the degreased product, mix the degreased produc...
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[0028] Example 1
[0029] The catalyst is alumina.
[0030] The extract is pulverized from orange peel to obtain the pulverized product. The pulverized product and petroleum ether are mixed according to a mass ratio of 1:7, and the extract is extracted at a temperature of 60° C. and 25r / min for 25 minutes.
[0031] The solid phase reagent is calcium carbonate.
[0032] A preparation method of a tableware disinfectant, the preparation method comprising the following steps:
[0033] (1) According to the mass ratio of 7:2:0.01, mix the soluble starch, dodecanol, and the catalyst, stir at 110℃, 200r / min for 1h, keep the vacuum at 0.01MPa for 1h, and adjust the pH to 8 After cooling to room temperature, filter to obtain the filter residue. According to the mass ratio of 1:3, the filter residue and hydrogen peroxide are mixed and decolorized for 1 hour, and filtered to obtain the decolorized product. The decolorized product is washed twice with ethanol and dried at a temperature of 50℃. Get...
Example Embodiment
[0038] Example 2
[0039] The catalyst is alumina.
[0040] The extract is pulverized from orange peel to obtain the pulverized product. The pulverized product and petroleum ether are mixed according to a mass ratio of 1:8, and the extract is extracted at a temperature of 70° C. and 30 r / min for 30 minutes.
[0041] The solid phase reagent is calcium bicarbonate.
[0042] A preparation method of a tableware disinfectant, the preparation method comprising the following steps:
[0043] (1) According to the mass ratio of 8:3:0.02, mix soluble starch, dodecanol, and catalyst, stir for 2h at a temperature of 120℃, 300r / min, and hold for 2h at a vacuum of 0.03MPa, and adjust the pH to 9 After cooling to room temperature, filter to obtain the filter residue. According to the mass ratio of 1:4, the filter residue and hydrogen peroxide are mixed and decolorized for 2 hours, filtered to obtain the decolorized product. The decolorized product is washed 3 times with ethanol and dried at a temperat...
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