Ilmenite-containing ilmenite separation beneficiation method

A beneficiation method and hematite technology, which is applied in the field of mineral processing, can solve the problems of inability to obtain ferro-titanium effectively, increase the difficulty of ilmenite ore, reduce the grade of titanium concentrate, etc., and achieve high titanium recovery rate and high production efficiency , the effect of low overall cost

Inactive Publication Date: 2018-07-06
NORTHEASTERN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, domestic research on titanium-containing hematite is less, not only because 95% of my country's titanium resources exist in primary vanadium-titanium magnetite ore, and there are few titanium-containing hematite resources; , specific magnetic susceptibility and electrical conductivity are close to those of ilmenite. Therefore, when using gravity separation, strong magnetic separation or electric separation to enrich ilmenite from iron dressing tailings, hematite will also enter titanium roughing In concentrate ore, this will not only fail to effectively separate ilmenite, but also increase the difficulty of subsequent purification of ilmenite
In addition, even in vanadium-titanium-magnetite deposits, there is also a small amount of hematite. When enriching ilmenite, this part of hematite will also enter the titanium concentrate, reducing the grade of titanium concentrate.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Titanium-containing hematite ore sample used, TiO 2 The content is 15.26%, and the TFe content is 45.85%.

[0033] The method proceeds as follows:

[0034] (1) The titanium-containing hematite ore sample is crushed to a particle size of -2.0mm, and the part that is ground to a particle size of -0.074mm accounts for 80% of the total weight of the material;

[0035] (2) Get the material after the ore grinding, and carry out magnetic separation by a strong magnetic separator under the magnetic field strength of 8500Gs to obtain a strong magnetic pre-selected coarse concentrate;

[0036] (3) Using a laboratory tubular roaster, the strong magnetic pre-selected coarse concentrate is reduced and roasted. The roasting temperature is 560 ° C. The mixed gas is a mixed gas composed of CO and nitrogen in a volume ratio of 3:7. The total gas volume of the mixed gas 0.015m 3 / h, the reduction roasting time is 10min, so that the weak magnetic hematite undergoes a reduction reaction...

Embodiment 2

[0040] Titanium-containing hematite ore sample used, TiO 2 The content is 16.53%, and the TFe content is 42.25%. The multi-element analysis results of raw materials are shown in Table 1.

[0041] Table 1

[0042] element

Fe

TiO 2

SiO 2

CaO

MgO

al 2 o 3

S

P

Content / wt%

42.25

16.53

8.98

0.04

0.47

8.03

0.03

[0043] The method proceeds as follows:

[0044] (1) Titanium-containing hematite is crushed to a particle size of -2.0mm, and the part that is ground to a particle size of -0.074mm accounts for 70% of the total weight of the material;

[0045] (2) Get the material after grinding, and carry out magnetic separation through the strong magnetic separator under the magnetic field intensity of 7500Gs, obtain the strong magnetic pre-selected rough concentrate;

[0046] (3) Using a suspension roaster, the strong magnetic pre-selected coarse concentrate is subjected to reduction roasting, the roast...

Embodiment 3

[0050] The titanium-containing hematite ore sample used, in which TiO 2 The content is 13.11%, and the TFe content is 48.82%. The method proceeds as follows:

[0051] (1) The titanium-containing hematite ore sample is crushed to a particle size of -2.0mm, and the ore is ground to a particle size of -0.074mm, and the content accounts for 75% of the total weight of the material;

[0052] (2) Get the material after grinding, and carry out magnetic separation by a strong magnetic separator under the magnetic field strength of 8000Gs to obtain strong magnetic pre-selected coarse concentrate;

[0053] (3) A laboratory tubular roaster is used to reduce and roast the strong magnetic pre-selected coarse concentrate. The roasting temperature is 580°C. The mixed gas is a mixed gas composed of CO and nitrogen in a volume ratio of 4:6. The total gas volume of the mixed gas 0.03m 3 / h, the reduction roasting time is 20min, so that the weak magnetic hematite undergoes a reduction reaction...

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Abstract

The invention relates to an ilmenite-containing ilmenite separation beneficiation method, and belongs to the field of mineral processing. The ilmenite-containing ilmenite separation beneficiation method comprises the following process steps that strong magnetic pre-selection is carried out on the titanium-containing hematite powder under the condition of the magnetic field intensity of 5000 Gs-13000 Gs, so as to obtain the titanium-iron mixed coarse concentrate; the titanium-iron mixed crude concentrate is roasted in a reducing atmosphere, wherein the roasting temperature is 500-620 DEG C, sothat the weakly-magnetic hematite is subjected to a reduction reaction to be converted into strong magnetic iron ore; cooling and grinding is carried out; and weak magnetic separation is carried out on the ground product under the condition that the magnetic field intensity is 750-1600 Gs, and the weak magnetic separation concentrate and the tailings are obtained. The method has the advantages ofhigh titanium recovery rate, high iron recovery rate, simple process structure and high production efficiency; and the comprehensive cost is low, the economical efficiency is good, the environment isprotected, the pollution is avoided, and the resources can be efficiently utilized, and the like.

Description

technical field [0001] The invention relates to a method for separating and beneficiating ilmenite minerals containing titanium hematite, which belongs to the field of mineral processing. Background technique [0002] Titanium and its alloys are widely used in the fields of aerospace, aviation and national defense because of their low density, high strength, high temperature resistance and corrosion resistance. In response to the growth of ore demand, it is of great practical significance to carry out research on the recovery and utilization of titanium resources. The primary ores are basically symbiotic ores, and there are different types of ilmenite, titanomagnetite and ilmenite. At present, the raw material of the titanium industry is mainly ilmenite, accounting for about 80% of the world's total titanium resources (according to TiO 2 calculate). At present, domestic research on titanium-containing hematite is less, not only because 95% of my country's titanium resourc...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B03C1/02B03C1/015C22B1/02C22B34/12
CPCB03C1/02B03C1/015C22B1/02C22B34/1209
Inventor 李文博韩跃新李艳军柳晓董振海
Owner NORTHEASTERN UNIV
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