Application of a high water-reducing and mud-resistant water-reducing agent in high-mud-content concrete
A technology of concrete and high mud content, which is applied in sustainable waste treatment, solid waste management, climate sustainability, etc. Dispersion, etc.
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Embodiment 1
[0052] An embodiment of the preparation method of the high water-reducing and mud-resistant water-reducing agent of the present invention comprises the following steps:
[0053] (1) Water, 3-buten-1-amine, H 3 PO 3 Add concentrated hydrochloric acid with a mass concentration of 37% into a 500ml four-neck glass flask with a stirrer, a thermometer, and a reflux condenser, fully stir and mix, heat up to 40°C, and slowly add formaldehyde solution with a mass concentration of 37%. The dropping time is controlled at 2 hours, and then the temperature is slowly raised to 75°C, and the reaction is continued for 2.5 hours to obtain the reaction monomer B;
[0054] (2) Water, APEG-CH 2 CH 2 NH 2 、H 3 PO 3 Add concentrated hydrochloric acid with a mass concentration of 37% into a 500ml four-necked glass flask equipped with a stirrer, a thermometer, and a reflux condenser, fully stir and mix, heat up to 40°C, slowly add a 37% formaldehyde aqueous solution dropwise, and drop The addi...
Embodiment 2
[0063] An embodiment of the preparation method of the high water-reducing and mud-resistant water-reducing agent of the present invention comprises the following steps:
[0064] (1) Water, 3-buten-1-amine, H 3 PO 3 Add concentrated hydrochloric acid with a mass concentration of 37% into a 500ml four-necked glass flask with a stirrer, a thermometer, and a reflux condenser, fully stir and mix, heat up to 45°C, and slowly add formaldehyde solution with a mass concentration of 37%. The dropping time is controlled at 1.5h, then the temperature is slowly raised to 85°C, and the reaction is continued for 1.5h to obtain the reaction monomer B;
[0065] (2) Water, HPEG-CH 2 CH 2 NH 2 、H 3 PO 3 Add concentrated hydrochloric acid with a mass concentration of 37% into a 500ml four-necked glass flask equipped with a stirrer, a thermometer, and a reflux condenser, fully stir and mix, heat up to 45°C, slowly add a 37% formaldehyde aqueous solution dropwise, and drop The addition time ...
Embodiment 3
[0074] An embodiment of the preparation method of the high water-reducing and mud-resistant water-reducing agent of the present invention comprises the following steps:
[0075] (1) Water, 3-buten-1-amine, H 3 PO 3 Add concentrated hydrochloric acid with a mass concentration of 37% into a 500ml four-necked glass flask with a stirrer, a thermometer, and a reflux condenser, fully stir and mix, heat up to 42°C, and slowly add formaldehyde solution with a mass concentration of 37%. The dropping time is controlled at 2 hours, and then the temperature is slowly raised to 80°C, and the reaction is continued for 2 hours to obtain the reaction monomer B;
[0076] (2) Water, TPEG-CH 2 CH2 NH 2 、H 3 PO 3 Add concentrated hydrochloric acid with a mass concentration of 37% into a 500ml four-necked glass flask equipped with a stirrer, a thermometer, and a reflux condenser, fully stir and mix, heat up to 43°C, slowly add a 37% formaldehyde aqueous solution dropwise, drop The addition t...
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