A kind of rubber material for wear-resistant tire and preparation method thereof
A technology for rubber materials and tires, applied in the field of rubber materials for wear-resistant tires and its preparation, can solve the problems that the wear resistance needs to be further improved, and achieve low requirements for equipment and reaction conditions, excellent flame retardancy, and easy-to-obtain raw materials Effect
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Embodiment 1
[0025] A rubber material for wear-resistant tires, which is prepared from the following components in parts by weight: 100 parts of cyanothiofluoroborosilicate rubber, 40 parts of modified epoxidized polybutadiene, 5 parts of molybdenum disulfide nanofibers, nano Grade ZSm-5 molecular sieve 15 parts.
[0026] The preparation method of the cyanothiofluoroborosilicate rubber comprises the following steps: 10 g of phenyl vinyl silicone oil, 10 g of 4-cyanostyrene, 10 g of perfluoro-n-propyl vinyl ether, 3 g of diallyl disulfide, 10 g of 1-(4-fluorophenyl) vinylboronic acid pinacol ester and 10 g of hexafluorobutyl methacrylate were dissolved in 100 g of dimethyl sulfoxide, then 0.1 g of azobisisobutyronitrile was added, and the Stirred and reacted at 60°C for 2 hours, then precipitated in water, washed 4 times with ethyl acetate, and then baked in a vacuum oven at 60°C for 10 hours to prepare cyanothiofluoroborosilicate rubber.
[0027] The preparation method of described modifi...
Embodiment 2
[0030] A rubber material for wear-resistant tires, prepared from the following components in parts by weight: 100 parts of cyanothiofluoroborosilicate rubber, 43 parts of modified epoxidized polybutadiene, 6 parts of molybdenum disulfide nanofibers, nano Grade ZSm-5 molecular sieve 16 parts.
[0031] The preparation method of the cyanothiofluoroborosilicate rubber comprises the steps of: mixing 10 g of phenylvinyl silicone oil, 10 g of 4-cyanostyrene, 10 g of perfluoro-n-propyl vinyl ether, and 3.5 g of diallyl disulfide , 10 g of 1-(4-fluorophenyl) vinylboronic acid pinacol ester, 10 g of hexafluorobutyl methacrylate were dissolved in 120 g of N,N-dimethylformamide, and then added azobisisoheptanonitrile 0.15g, under nitrogen atmosphere, stirred and reacted at 63°C for 2.3 hours, then precipitated in water, washed 5 times with ethyl acetate, and then baked in a vacuum oven at 65°C for 12 hours to prepare boron cyanthiofluoride Silicone Rubber.
[0032] The preparation metho...
Embodiment 3
[0035]A rubber material for wear-resistant tires, prepared from the following components in parts by weight: 100 parts of cyanothiofluoroborosilicate rubber, 45 parts of modified epoxidized polybutadiene, 7 parts of molybdenum disulfide nanofibers, nano Grade ZSm-5 molecular sieve 17 parts.
[0036] The preparation method of the cyanothiofluoroborosilicate rubber comprises the following steps: 10 g of phenyl vinyl silicone oil, 10 g of 4-cyanostyrene, 10 g of perfluoro-n-propyl vinyl ether, 4 g of diallyl disulfide, 10g of 1-(4-fluorophenyl)vinylboronic acid pinacol ester and 10g of hexafluorobutyl methacrylate were dissolved in 135g of N-methylpyrrolidone, and then 0.16g of azobisisobutyronitrile was added. Under the atmosphere, stirred and reacted at 65°C for 2.5 hours, then precipitated in water, washed 6 times with ethyl acetate, and then baked in a vacuum oven at 70°C for 12 hours to prepare cyanothiofluoroborosilicate rubber.
[0037] The preparation method of the modif...
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