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Method for preparing high-adhesion wear-resistant paint used for polycarbonate

A high-adhesion, wear-resistant coating technology, applied in coatings and other directions, can solve the problems of poor crack growth resistance, weather resistance, low surface hardness, and poor wear resistance, so as to enhance interaction and bonding strength and improve wear resistance. , Improve the effect of surface free energy

Inactive Publication Date: 2018-07-27
SUZHOU FUZHONG PLASTIC CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, PC also has the problems of low surface hardness, poor wear resistance, easy to scratch, chemical solvent resistance, crack growth resistance and poor weather resistance.

Method used

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  • Method for preparing high-adhesion wear-resistant paint used for polycarbonate

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] A preparation method for polycarbonate with high adhesion wear-resistant paint, comprising the following steps:

[0018] S1. Weigh the following ingredients by weight: 30 parts of chlorinated polypropylene resin, 35 parts of maleic anhydride modified C5 petroleum resin, 1.2 parts of BYK-163 type dispersant, 0.6 part of BYK-071 type defoamer, dilaurel 0.05 parts of dibutyltin acetate, 4 parts of cellulose acetate butyrate, 14 parts of xylene, 16 parts of ethyl acetate, 18 parts of isopropanol, 3 parts of aliphatic polyisocyanate, 5 parts of white corundum micropowder, 1 part of superfine mica powder, silane 0.5 parts of coupling agent KH-560, 8 parts of porous spherical silica;

[0019] S2. Mix chlorinated polypropylene resin and maleic anhydride modified C5 petroleum resin, stir for 5 minutes, add BYK-163 type dispersant, BYK-071 type defoamer, dibutyltin dilaurate, butyl acetate under stirring state Acid cellulose, white corundum micropowder, ultrafine mica powder and...

Embodiment 2

[0021] A preparation method for polycarbonate with high adhesion wear-resistant paint, comprising the following steps:

[0022] S1. Weigh the following ingredients by weight: 42 parts of chlorinated polypropylene resin, 18 parts of hydroxy-modified vinyl acetate resin, 1.8 parts of BYK-163 type dispersant, 0.2 parts of BYK-071 type defoamer, dilauric acid 0.08 parts of dibutyltin, 8 parts of cellulose acetate butyrate, 25 parts of isopropanol, 18 parts of ethyl acetate, 17 parts of butyl acetate, 8 parts of aromatic polyisocyanate, 2 parts of white corundum micropowder, 3 parts of superfine mica powder , 1.2 parts of silane coupling agent KH-570, 4 parts of porous spherical zirconium silicate, wherein, the preparation method of hydroxyl-modified vinyl acetate resin is to mix methanol and sodium hydroxide, heat to 35 ° C in a water bath, and stir for 20 min Afterwards, add vinyl acetate, react 8h, remove mother liquor and wash and filter to obtain hydroxyl-modified vinyl acetat...

Embodiment 3

[0025] A preparation method for polycarbonate with high adhesion wear-resistant paint, comprising the following steps:

[0026] S1. Weigh the following ingredients by weight: 35 parts of chlorinated polypropylene resin, 9 parts of maleic anhydride modified C5 petroleum resin, 19 parts of hydroxyl modified vinyl acetate resin, 1.4 parts of BYK-163 dispersant, BYK-071 0.3 parts of antifoaming agent, 0.07 parts of dibutyltin dilaurate, 7 parts of cellulose acetate butyrate, 15 parts of ethyl acetate, 30 parts of isopropanol, 12 parts of methyl isobutyl ketone, 5 parts of aliphatic polyisocyanate , 3 parts of white corundum micropowder, 3 parts of superfine mica powder, 0.7 parts of silane coupling agent KH-550, 4 parts of porous spherical silica, 3 parts of porous spherical zirconium silicate, of which, hydroxyl modified chloroacetic acid The resin preparation method is to mix methanol and sodium hydroxide, heat to 45°C in a water bath, and stir for 10 minutes, then add chloroace...

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Abstract

The invention provides a method for preparing a high-adhesion wear-resistant paint used for polycarbonate. The method comprises the following steps: chlorinated polypropylene resin and modified resinare mixed, and stirred for 5-10 min, a BYK-163 type dispersant, a BYK-071 type antifoaming agent, dibutyltin dilaurate, cellulose acetate butyrate, corundum micro powder, ultrafine mica powder and a porous inorganic particle material are added under a stirring state, a sand milling machine is used for grinding the materials with fineness being less than or equal to 25 [mu]m, a solvent is added, the materials are heated to the temperature of 30-40 DEG C and is subjected to heating backflow for 1h, a silane coupling agent and a curing agent are added, cooling is carried out to room temperature,and the solvent is used for dilution. The paint has high adhesion, water resistance and excellent wear resistance.

Description

technical field [0001] The invention relates to the field of plastic coatings, in particular to a preparation method of a high-adhesion wear-resistant coating for polycarbonate. Background technique [0002] Polycarbonate (PC) is an important optical thermoplastic resin, which has the advantages of high transparency, good impact resistance, low density, low price and easy processing. Not only is it widely used in the production of transparent parts such as plates, eye lenses, and automobile windshields, but it has also been the first choice for high-speed aircraft in developed countries to improve the high-temperature resistance and bird impact resistance of transparent parts. However, PC also has the problems of low surface hardness, poor wear resistance, easy to scratch, chemical solvent resistance, crack growth resistance and poor weather resistance. The surface free energy of polycarbonate sheets is generally lower than that of metal surfaces, and even the surface tensi...

Claims

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Application Information

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IPC IPC(8): C09D151/00C09D123/28C09D127/22C09D7/61C09D7/63C09D7/65
Inventor 史闵新
Owner SUZHOU FUZHONG PLASTIC CO LTD
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