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A kind of preparation method and application of water-insoluble xylan

A water-insoluble xylan technology, applied in the field of food science, can solve problems such as lye recovery, large alcohol loss, and unclear separation and purification, so as to prevent fatty liver disease, regulate intestinal flora, Improvement effect of muddy soup phenomenon

Active Publication Date: 2021-04-27
谷创芯生物科技(厦门)有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0013] Although patent 1 can prepare xylan in a large amount from agricultural wastes and provide raw materials for the production of xylooligosaccharides, xylose, and xylitol, there are several deficiencies. 1. The xylan extract has no effect on Alkali is recycled but directly neutralized, which has high cost and large amount of waste water; 2. The impurity separation and purification process completely depends on the alcohol precipitation method. The xylan purification and purification process is exposed to alcohol, and the removal of water-soluble impurities is not complete; 3. Water-soluble wood Glycans and water-insoluble xylans are not isolated and xylan purity is not addressed
[0014] Although the method for preparing plant xylan by improved alkaline extraction in Patent 2 effectively reduces the production cost of xylan products and significantly improves the social and economic benefits of industrial production of plant fiber xylan, there are several shortcomings and have not yet been developed. What is clear, 1. Only use the method of recycling the extract to save alkali consumption per unit of xylan, and there is no mention of the recovery of the lye in the extract; 2. It is not stated that the alkali concentration of the extract is reduced from 5%-7% to Whether the pH12.0 is removed by direct acid neutralization or ultrafiltration membrane replacement; 3. Under the initial condition of the extract pH12.0, the purpose of using soft water ultrafiltration membrane replacement is to remove residual alkali or to separate and purify impurities. Clear; 4. The purity of xylan after soft water ultrafiltration membrane replacement only increased from 70% of the traditional process to 75%, and the deep separation and purification process of impurities still relies on alcohol precipitation or washing; 5. There is no mention of water-soluble xylan and water How to separate insoluble xylan
[0015] In the above-mentioned patents, the purification of xylan adopts the traditional method of alcohol precipitation, but the alcohol precipitation method requires high equipment safety, large amount of alcohol loss, high cost, and incomplete removal of water-soluble impurities.

Method used

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  • A kind of preparation method and application of water-insoluble xylan
  • A kind of preparation method and application of water-insoluble xylan
  • A kind of preparation method and application of water-insoluble xylan

Examples

Experimental program
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Effect test

Embodiment 1

[0049] The preparation method of water-insoluble xylan comprises the following steps:

[0050] 1) Take 100 parts by weight of non-mildew and dry sugarcane straw raw materials, put them into 600 parts by weight of clean water and soak for 2 hours, use a press to remove free water, then soak the sugarcane straw raw materials again and squeeze them dry to obtain clean sugarcane The straw raw material is controlled to have a moisture content of 50%; the cleaned sugarcane straw raw material is put into 800 parts by weight of a sodium hydroxide solution with a mass concentration of 9%, mechanically ground under alkaline conditions, centrifuged and precipitated for solid-liquid Separation to obtain centrifuged residue and extract lye; the centrifuged residue is washed twice with a sodium hydroxide solution with a mass concentration of 6%, and solid-liquid separation is carried out each time;

[0051] 2) Merge three extractions of lye, and use an alkali-resistant ultrafiltration membr...

Embodiment 2

[0057] The preparation method of water-insoluble xylan comprises the following steps:

[0058]1) Take 100 parts by weight of non-mildew and dry corn stalk raw material, put it into 600 parts by weight of clean water and soak for 2 hours, use a press to remove free water, then soak the corn stalk raw material again and squeeze it dry to obtain washed corn The straw raw material is controlled to have a moisture content of 50%; the cleaned corn stalk raw material is put into 1100 parts by weight of a sodium hydroxide solution with a mass concentration of 9%, mechanically ground under alkaline conditions, centrifuged and precipitated for solid-liquid Separation to obtain centrifuged residue and extract lye; the centrifuged residue is washed twice with a sodium hydroxide solution with a mass concentration of 6%, and solid-liquid separation is carried out each time;

[0059] 2) Merge the lye extracted three times, and use an alkali-resistant ultrafiltration membrane with a molecular...

Embodiment 3

[0065] The preparation method of water-insoluble xylan comprises the following steps:

[0066] 1) Take 100 parts by weight of non-mildew and dry wheat straw raw materials, soak them in 600 parts by weight of clean water for 2 hours, use a press to remove free water, soak the raw materials of wheat straws in water again and squeeze them dry to obtain washed wheat The straw raw material is controlled to have a moisture content of 50%; the cleaned wheat straw raw material is put into 1400 parts by weight of a sodium hydroxide solution with a mass concentration of 9%, mechanically ground under alkaline conditions, centrifuged and precipitated for solid-liquid Separation to obtain centrifuged residue and extract lye; the centrifuged residue is washed twice with a sodium hydroxide solution with a mass concentration of 6%, and solid-liquid separation is carried out each time;

[0067] 2) Merge the lye extracted three times, and use an alkali-resistant ultrafiltration membrane with a ...

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Abstract

The invention discloses a preparation method and application of water-insoluble xylan, that is, the xylan in the plant cell wall is extracted with lye, and the water-insoluble part after removing most of the lye is deeply purified and bleached. treatment to obtain edible water-insoluble xylan, in which impurities are separated and purified by using dilute alkaline water with a specific pH value for multiple replacement ultrafiltration, adjusting the pH value of the emulsion to 8‑13 with acid, and then using centrifugation or micro The filter membrane is replaced and washed without using alcohol in the whole process. The product is only water-insoluble xylan, and the soluble part is completely removed. The purity content can reach 85%‑90%. The water-insoluble xylan prepared by the method of the invention has the effects of promoting intestinal health, inhibiting starch decomposition and absorption, lowering serum cholesterol, lowering serum triglyceride, eliminating constipation, eliminating fatty liver and improving the processing performance of rice noodle food.

Description

technical field [0001] The invention belongs to the field of food science, and relates to extracting xylan in plant cell walls with lye, removing most of the water-insoluble part of lye, and obtaining edible water-insoluble xylan after deep purification and bleaching treatment. sugar. Background technique [0002] The development of modern agriculture and animal husbandry has provided people with more cheap food and meat products. The human diet in the past few million years has been replaced by a high-fat, high-protein and increasingly refined diet. , directly lead to a serious shortage of dietary fiber components in human plant foods—that is, plant non-starch polysaccharides in foods, which has become an important cause of many metabolic diseases. [0003] The human body lacks dietary fiber hydrolytic enzymes and cannot directly hydrolyze, absorb and utilize dietary fiber in the small intestine. After ingestion, dietary fiber is mainly used as the basic carbon source for ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08B37/00A23L33/125A23L29/30A23L7/10A61K31/715A61P3/06A61P1/10A61P1/16
CPCA23V2002/00A61K31/715A23L7/10A23L29/30A23L33/125A61P1/10A61P1/16A61P3/06C08B37/0003C08B37/0057A23V2200/3262A23V2200/3202A23V2200/32A23V2200/30A23V2250/51
Inventor 代兴华石国良张永昌林卫军张永宁卢艺芳王羽娟张厚瑞陈海珊陈建军李赐玉覃香香周玉恒蔡爱华
Owner 谷创芯生物科技(厦门)有限公司