Steel pipe drawing emulsified oil with ultrahigh lubricating property and preparation method thereof

A technology of lubricating performance and emulsified oil, used in lubricating compositions, petroleum industry and other directions, can solve the problems of surface finish, brightness reduction, bad influence of heat treatment and annealing quality, and lack of matching lubricating oil for welded pipes. Not easy to deteriorate, prevent sintering, and easy to operate

Active Publication Date: 2018-08-17
NANJING INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the steel pipe drawing lubricating oil has the problem of poor lubrication and cooling effect. After the steel pipe has been drawn many times, a large amount of metal powder is bonded to the surface of the drawn pipe and the edge of the hole core, resulting in a sharp increase in the friction coefficient between the two. Large, not only sharply reduce the surface finish and brightness of the drawn workpiece, but also aggravate the wear of the mold and affect the service life of the mold
In recent years, welded steel pipes have developed rapidly due to the advantages of simple production process, high production efficiency, low cost, high precision, uniform wall thickness, and arbitrary size. However, welded pipes do not have matching lubricating oil, and often Occurrence of quality problems of weld cracking due to local overheating of the steel pipe or mold
In addition, the currently used drawing lubricating oil is not easy to clean, which will have a negative impact on the heat treatment and annealing quality of the drawn steel pipe.

Method used

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  • Steel pipe drawing emulsified oil with ultrahigh lubricating property and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] The formula of Example 1 is shown in the following table:

[0017] Serial number

[0018] Production method: According to the weight formula of each component in the above table, first put 120kg palm oil and 740kg mechanical oil N68 into a reactor at a speed of 50-120 revolutions per minute for heating and stirring. When the temperature reaches 60-80°C, then sequentially 2kg oil-soluble nano Fe 3 O 4 (2-50nm), 4kg nitrogen-containing borate, 2kg zinc dialkyl dithiophosphate, 30kg butyl stearate, 30kg C8-C10 mixed alcohol, 3kg sodium dodecylbenzene sulfonate and 3kg dimercaptothiol Diazole was added to the reaction kettle, kept warm and continuously stirred for 60-100 minutes, and then when the temperature dropped to 70°C, add 20kg sorbitan oleate Span80, 20kg nonylphenol polyoxyethylene ether, 20kg triethanolamine, 3kg of methyl silicone oil and 3kg of pentachloronitrobenzene, adjust the speed of the mixer to 30 rpm and keep stirring for 30-60 minutes, then stop heating...

Embodiment 2

[0020] The production method is the same as in Example 1, and the component names and their weight percentages are shown in the following table:

[0021] Serial number

[0022] Production method: According to the weight formula of each component in the above table, first put 150kg palm oil and 390kg mechanical oil N68 into a reactor at a speed of 50-120 revolutions per minute for heating and stirring. When the temperature reaches 60-80°C, then sequentially 10kg oil-soluble nano Fe 3 O 4 (2-50nm), 20kg nitrogen-containing borate, 30kg zinc dialkyl dithiophosphate, 60kg butyl stearate, 80kg C8-C10 mixed alcohol, 20kg sodium dodecylbenzene sulfonate and 15kg dimercaptothiol Diazole was added to the reactor, kept warm and continuously stirred for 60-100 minutes, and then when the temperature dropped to 70°C, 50kg sorbitan oleate Span80, 40kg nonylphenol polyoxyethylene ether, 80kg triethanolamine, 25kg methyl silicone oil and 30kg pentachloronitrobenzene, adjust the mixer speed to...

Embodiment 3

[0024] The formula of Example 3 is shown in the following table:

[0025] Serial number

Component name

Weight percentage (100%)

1

Oil-soluble nano Fe 3 O 4 (2-50nm)

15

2

Nitrogen-containing borate

30

3

Zinc dialkyl dithiophosphate

45

4

Butyl Stearate

100

5

C8-C10 mixed alcohol

80

6

Sorbitan Oleate Span80

60

7

Polyoxyethylene nonylphenol ether

60

8

Triethanolamine

100

9

Sodium dodecyl benzene sulfonate

30

10

Dimercaptothiadiazole

20

11

Pentachloronitrobenzene

30

12

Methyl silicone oil

40

13

Palm oil

180

14

Mechanical oil N68

210

[0026] Production method: According to the weight formula of each component in the above table, first put 180kg palm oil and 210kg mechanical oil N68 into a reactor at a speed of 50-120 revolutions per minute for heating and stirring. When the temperature reaches 60-80°C, then sequentially Put 15kg oil-soluble nano Fe 3 O 4 (2-50nm), 30kg nitrogen-containing borate, 45kg zinc dialkyl dithiophosphate, 100kg butyl stearate, 80kg C8-C10 mixed alcohol, ...

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PUM

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Abstract

The invention relates to a steel pipe drawing emulsified oil with ultrahigh lubricating property and a preparation method thereof. The method comprises the following steps: palm oil and machine oil N68 are first poured into a reaction kettle at the rotational speed of 50 to 120 rotations per minutes, heated and agitated; when temperature reaches 60 DEG C to 80 DEG C, oil-soluble nano Fe3O4 (2nm to50nm), nitrogen-containing borate, zinc dialkylphosphorodithiloate, butyl stearate, C8-C10 mixed alcohol, sodium dodecyl benzene sulfonate and dimercaptothiodiazole are then sequentially added into the reaction kettle, and agitation is continued for 60 to 100 minutes while temperature is kept; afterwards, when temperature is decreased to 70 DEG C, sorbitan monooleate Span 80, nonyl phenol polyoxyethylene ether, triethanolamine, methylsilicone oil and quintozene are added, the rotational speed of an agitator is adjusted to 30 rotations per minutes and agitation is kept for 30 to 60 minutes, heating is then stopped, agitation is continued until room temperature is reached, and thereby the welded pipe drawing emulsified oil which is yellowish-brown, transparent and uniform is obtained. The product disclosed by the invention is easy to degrade, the anticorrosive period is longer, the annealing detergency is better, and moreover, environment pollution can be reduced.

Description

Technical field [0001] The invention relates to the technical field of lubricants and is used for lubrication in the cold drawing process of various steel pipes such as stainless steel and high-temperature alloys, especially welded pipes. Specifically, it is a steel pipe drawing emulsified oil with ultra-high lubricating performance and the same The preparation method can prevent the welded pipe from being locally overheated during the cold drawing process to cause weld cracking, oxidation and discoloration, and can ensure the steel pipe drawing emulsified oil of the finished surface brightness. Background technique [0002] The drawing process is a typical plastic processing method in which the cross-sectional area of ​​the metal processing material is reduced through the die core under the drawing action to obtain high-precision, high-finish wire or pipe. In the drawing process, due to the large amount of metal deformation and the continuous production of new friction surfaces,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M169/04C10N30/06C10N40/24C10N50/00C10N30/12
CPCC10M169/048C10M2201/062C10M2203/1006C10M2207/021C10M2207/281C10M2207/289C10M2207/401C10M2209/104C10M2209/108C10M2215/042C10M2215/202C10M2219/044C10M2219/106C10M2223/045C10M2227/061C10M2229/041C10N2030/06C10N2030/12C10N2040/24C10N2030/56C10N2040/246C10N2050/01C10N2020/06C10N2020/093C10N2010/02C10N2010/04
Inventor 熊桑王章忠初雅杰王珏毛向阳
Owner NANJING INST OF TECH
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