Sugar palm analgesic extract and preparation method and use thereof

A technology of extract and sugarcane, applied in the field of sugarcane analgesic extract and preparation thereof, can solve the problems of small application range of sugarcane extract, poor pain relief effect of sugarcane extract chelidonate, etc., and avoid macropores. Effects of resin overloading, increasing foot pain threshold, and increasing productivity

Active Publication Date: 2021-07-13
王伟明
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Therefore, the technical problem to be solved in the present invention is to overcome the problems in the prior art that the analgesic effect of sugar palm extract chelidinate is not good and the application range of sugar palm is small, thereby providing a sugar palm pain-relieving extract and its preparation method and use

Method used

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  • Sugar palm analgesic extract and preparation method and use thereof
  • Sugar palm analgesic extract and preparation method and use thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Embodiment 1 (claim 1)

[0027] (1) Put 1 kg of sugarcane fruit in a pulverizer and grind it to 60 mesh, then add 1.5L of ethanol solution with a concentration of 65% and soak for one day, recover the soaking solution, and add 1.5L of 65% ethanol solution to the sugarcane fruit again. % ethanol solution for immersion for one day, and combine the two immersion solutions to obtain the extract;

[0028] (2) Concentrate the above extract under reduced pressure at 60°C for 2 hours to remove ethanol to obtain an extract, measure the relative density of the extract to be 1.25, then add water to the extract and stir continuously, and measure with a hydrometer at the same time until the relative density is obtained 1.10 extract dilution;

[0029] (3) Adopt the macroporous resin that model is R8-18 to extract the medicinal extract dilution that obtains through macroporous adsorption resin, be 100:20 (g / g) respectively according to the consumption of macroporous resin consumption...

Embodiment 2

[0030] Embodiment 2: (increase alcohol precipitation)

[0031] (1) Put 1 kg of sugarcane fruit in a pulverizer and grind it to 55 mesh, then add 1.5L of ethanol solution with a concentration of 65% and soak for one day, recover the soaking solution, and add 1.5L of 65% ethanol solution to the sugarcane fruit again. % ethanol solution for immersion for one day, and combine the two immersion solutions to obtain the extract;

[0032] (2) The extract was concentrated under reduced pressure at 60°C for 2 hours to remove ethanol to obtain an extract, and the extract obtained was first added to 3L of 95% ethanol solution in volume, left to stand for 24 hours, and the precipitate was removed to get the supernatant of the extract. Measure the relative density of the supernatant of the extract to be 1.25, then add water to the supernatant of the extract and stir continuously, while measuring with a hydrometer until obtaining a dilution of the extract with a relative density of 1.10;

...

Embodiment 3

[0034] Embodiment 3: (increase ultrafiltration)

[0035] (1) Put 1 kg of sugarcane fruit in a pulverizer and grind it to 50 mesh, then add 1.5L of ethanol solution with a concentration of 65% and soak for one day, recover the soaking solution, and add 1.5L of 65% ethanol solution to the sugarcane fruit again. % ethanol solution for immersion for one day, and combine the two immersion solutions to obtain the extract;

[0036] (2) Concentrate the extract under reduced pressure at 60°C for 2 hours to remove ethanol to obtain the extract, measure the relative density of the supernatant of the extract to be 1.25, then add water to the supernatant of the extract and stir continuously, while using the specific gravity Meter measurement, until obtaining relative density is the medicinal extract dilution of 1.10, then above-mentioned medicinal extract dilution is ultrafiltered by the ultrafiltration tube that molecular weight cut off is 3000, and the relative density of the medicinal ext...

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Abstract

A preparation method of sugarcane analgesic extract, comprising the following steps: (1) slicing or pulverizing sugarcane fruit, refluxing or soaking in ethanol solution to obtain ethanol extract; (2) preparing The ethanol in the ethanol extract is removed to obtain the extract, which is diluted with water to obtain a dilution of the extract with a relative density of 1.02-1.21; (3) the above dilution of the extract is extracted by a macroporous adsorption resin, followed by water and / or ethanol After the solution washes the resin, it is eluted with 60%-95% ethanol solution, the eluate is collected until it is colorless, concentrated under reduced pressure, and the sugar palm analgesic extract is obtained. The sugar palm analgesic extract obtained by this final preparation method has good analgesic properties effect and higher productivity.

Description

technical field [0001] The invention relates to the field of medicine, in particular to sugar palm analgesic extract and its preparation method and application. Background technique [0002] Sugar palm (scientific name: Arenga pinnata (Wurmb.) Merr.), Palmaceae tree, the thorn is relatively strong, 5 meters to 10 meters high, the fruit matures about 2-3 years after flowering, the fruit is nearly spherical, 5-6cm long, 4-5cm in diameter, dark brown outer surface, with white fine hairs, obvious bumps formed by shriveling, and 3 persistent perianths at the base, wide at the bottom and narrow at the top. Sugar palm is a common plant in the south, with a wide distribution and a huge amount of fruit. Sugar palm is generally made into edible products such as sugar palm powder, sugar palm oil tea, sugar palm wine or sugar palm sugar, but its application in the field of medicine has not yet been rationalized. develop. [0003] Among them, the Chinese invention patent with the publi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K36/889A61P29/00A61P25/02A61K131/00
CPCA61K36/889A61K2236/333A61K2236/51A61K2236/53A61K2236/55A61P25/02A61P29/00
Inventor 王伟明黄璐琦霍金海王昶李凤金庄岩孙国东
Owner 王伟明
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