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A kind of polyoxyethylene ether betaine polycarboxylic acid sodium salt and preparation method thereof

A technology of sodium polycarboxylate and polyoxyethylene ether, which is applied in dyeing, ampholyte/electroneutral surface active compounds, textiles and papermaking, and can solve the trend and toxicity that do not meet the requirements of environmentally friendly green surfactants , heavy smell of benzyl chloride and other problems, to achieve a good prospect of large-scale promotion and use in the market, and to improve the effect of hardness

Active Publication Date: 2020-12-15
苏州联胜化学有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0007] But this anti-staining soaping agent does not meet the trend of current society's demand for environmentally friendly green surfactants due to the following reasons:
[0008] 1. Benzyl chloride has a very strong smell, and chloroethanol is highly toxic to the human body;

Method used

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Effect test

Embodiment 1

[0042] One embodiment of the present invention provides a polyoxyethylene ether betaine polycarboxylate sodium salt, its raw material components include: 65 parts of fatty amine polyoxyethylene ether, 26 parts of carboxylation reagent, 23 parts of quaternization reagent, 43 parts of solvent, 15 parts of alkali agent, 1 part of pH regulator and 0.3 part of phase transfer catalyst.

[0043] The fatty amine polyoxyethylene ether structure is C X h 2X+3 N(EO) Y (EO) Z , wherein X=12; Y+Z=15; the carboxylation reagent is maleic anhydride; the quaternization reagent is chloroacetic acid; the solvent includes deionized water, ethanol, ethylene glycol monobutyl ether; the alkali agent is sodium hydroxide; the pH regulator is citric acid and sodium carbonate; the phase transfer catalyst is tetrabutylammonium bromide.

[0044] Its preparation method comprises the following steps:

[0045] Add the aliphatic amine polyoxyethyl ether ether into a four-necked flask equipped with a ther...

Embodiment 2

[0052] Another embodiment of the present invention provides a polyoxyethylene ether betaine polycarboxylate sodium salt, its raw material components include: 72 parts of fatty amine polyoxyethylene ether, 27 parts of carboxylation reagent, 21 parts of quaternization reagent , 45 parts of solvent, 16 parts of alkali agent, 1 part of pH regulator, 0.3 part of phase transfer catalyst.

[0053] Wherein the fatty amine polyoxyethylene ether structure is C X h 2X+3 N(EO) Y (EO) Z , wherein X=18; Y+Z=20; the carboxylation reagent is maleic anhydride and phthalic anhydride mixed in a weight ratio of 2:1; the quaternization reagent is sodium chloroacetate; the solvent It includes ethanol, deionized water and ethylene glycol monobutyl ether; the alkali agent is sodium hydroxide; the pH regulator is citric acid and sodium carbonate; the phase transfer catalyst is tetrabutylammonium bromide.

[0054] Its preparation method comprises the following steps:

[0055] Add the aliphatic amine...

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Abstract

The invention provides polyoxyethylene ether betaine polycarboxylate sodium salt and a preparation method thereof. The polyoxyethylene ether betaine polycarboxylate comprises 60-75 parts of fatty amine polyoxyethylene ether, 25-30 parts of carboxylic acid reagent, 20-25 parts of quaternizing reagent, 40-50 parts of solvent, 12-18 parts of alkali agent, 0.5-2 parts of pH adjuster, and 0.1-0.5 partof phase transfer catalyst. The invention relates to the polyoxyethylene ether betaine polycarboxylate sodium salt, and the polyoxyethylene ether betaine polycarboxylate sodium salt contains a betainezwitterionic surfactant which has no irritation to a human body and is green, environmentally friendly and biodegradable, so that environmental protection throughout the process from raw material production, finished product use and final emission is achieved.

Description

technical field [0001] The invention relates to an anti-staining soaping agent used in textile dyeing and finishing industry, which is used in textile printing and dyeing or printing. Background technique [0002] It is known that the printing and dyeing industry is an important component of the textile industry, and it is also an industry with high energy consumption and large sewage discharge. With the continuous development of society, environmental issues are getting more and more attention from the society, and the corresponding calls for environmental protection are getting higher and higher. Therefore, the official requirements for energy conservation, environmental protection and emission reduction of enterprises are also getting higher and higher. [0003] For the printing and dyeing industry, in addition to research and development of high-efficiency, water-saving, and energy-saving equipment, and the development and promotion of practical new technologies for ener...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08G65/337C08G65/331D06P5/08D06P5/06D06P1/66C11D1/90
CPCC08G65/331C08G65/337C11D1/90D06P1/66D06P5/06D06P5/08
Inventor 李正生涂胜宏
Owner 苏州联胜化学有限公司
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