Preparation method of polyaniline conductive film
A technology of conductive film and polyaniline, which is applied in the field of preparation of polyaniline conductive film, can solve the problems of poor uniformity and stability of the film, lower quality of conductive film, and poor stability of finished products, so as to improve storage stability and conduction stability , Improve the effect of tensile strength
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Embodiment 1
[0023] (1) Take sodium persulfate, add it to deionized water 30 times its weight, and stir evenly to obtain an aqueous initiator solution;
[0024] (2) Take the silane coupling agent kh560, add it to anhydrous ethanol 13 times its weight, raise the temperature to 60°C, add dodecyl mercaptan, keep stirring for 20 minutes, and obtain a composite silane solution;
[0025] (3) Take stearic acid, heat and melt it, mix it with light calcium carbonate, add it to deionized water 70 times the weight of the mixture, ultrasonicate it for 10 minutes, mix it with the above compound silane solution, and send it into the reaction kettle to control the reaction The pressure of the kettle is 1mpa, the elevated temperature is 95°C, the temperature is kept and stirred for 2 hours, the discharge is cooled, centrifuged, and the precipitate is dried to obtain organically modified calcium carbonate;
[0026] (4) Take polytetrafluoroethylene wax, add it to the solvent, and stir evenly to obtain a wax...
Embodiment 2
[0033] (1) Take ammonium persulfate, add it to deionized water 25 times its weight, and stir evenly to obtain an aqueous initiator solution;
[0034] (2) Take the silane coupling agent kh560, add it to anhydrous ethanol 10 times its weight, raise the temperature to 55°C, add dodecyl mercaptan, keep stirring for 4 minutes, and obtain a composite silane solution;
[0035] (3) Take stearic acid, heat and melt, mix with light calcium carbonate, add to deionized water 60 times the weight of the mixture, ultrasonicate for 5 minutes, mix with the above compound silane solution, and send it into the reaction kettle to control the reaction The pressure of the kettle is 0.9mpa, the elevated temperature is 90°C, the temperature is kept and stirred for 1 hour, the discharge is cooled, centrifuged, and the precipitate is dried to obtain organically modified calcium carbonate;
[0036] (4) Take polytetrafluoroethylene wax, add it to the solvent, and stir evenly to obtain a wax solvent;
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