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Waterborne aromatic polyisocyanate cross-linking agent and preparation method thereof

A technology of polyisocyanate and diisocyanate, which is applied in the field of water-based aromatic polyisocyanate crosslinking agent and its preparation, can solve the problems of low activity and poor practical effect, achieve low film forming temperature, facilitate the summary of production experience, and stabilize Good results

Inactive Publication Date: 2018-09-28
上海浩登材料股份有限公司 +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The technical problem to be solved in the present invention is to provide a water-based aromatic polyisocyanate crosslinking agent to solve the problems of low activity and poor practical effect in the prior art.

Method used

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  • Waterborne aromatic polyisocyanate cross-linking agent and preparation method thereof
  • Waterborne aromatic polyisocyanate cross-linking agent and preparation method thereof
  • Waterborne aromatic polyisocyanate cross-linking agent and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0032] A water-based aromatic polyisocyanate crosslinking agent, which comprises the following components by mass percentage:

[0033] Fatty alcohol polyoxyethylene ether 3~10%, polyisocyanate 10%, methylenesuccinic acid 3%, polyether polyurethane 8%, isophorone diamine 4%, glycidyl methacrylate 8%, acrylic acid 10% of ester, 5% of styrene, 8% of isopropanol, 3% of auxiliary agent and the balance are deionized water.

[0034] In this embodiment, the polyisocyanate is any one of diisocyanate, isophorone diisocyanate, bicyclic and methane diisocyanate, and tetramethylbenzene dimethylene diisocyanate.

[0035] In this embodiment, the auxiliary agent is composed of the following raw materials by weight, wherein 1% of silane coupling agent, 3% of TAC, 10% of styrene, 20% of phytate, 3% of neopentyl glycol, Antioxidant 1%, diethylene glycol 5%, and the balance ethanol.

[0036] In this embodiment, the antioxidants are polymers of 2-acetone and N-phenylaniline, tris(nonylphenol) ph...

Embodiment 2

[0043] A water-based aromatic polyisocyanate crosslinking agent, which comprises the following components by mass percentage:

[0044] Fatty alcohol polyoxyethylene ether 310% (the percentage here seems wrong, please confirm), polyisocyanate 10%, methylene succinic acid 3%, polyether polyurethane 1%, isophorone diamine 2%, methyl Glycidyl acrylate 5%, acrylate 5%, styrene 10%, auxiliary agent 5% and the balance is deionized water.

[0045] In this embodiment, the polyisocyanate is any one of diisocyanate, isophorone diisocyanate, bicyclic and methane diisocyanate, and tetramethylbenzene dimethylene diisocyanate.

[0046] In this example, the auxiliary agent is composed of the following raw materials by weight, wherein 3% of silane coupling agent, 3% of TAC, 4% of styrene, 35% of phytate, 3% of neopentyl glycol, 3% of anti- Oxidant 5%, diethylene glycol 10%, and the balance ethanol.

[0047] In this embodiment, the antioxidants are polymers of 2-acetone and N-phenylaniline, t...

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Abstract

The invention discloses a waterborne aromatic polyisocyanate cross-linking agent. The waterborne aromatic polyisocyanate cross-linking agent comprises the following components in percentages by mass:3 to 10% of fatty alcohol-polyoxyethylene ether, 10 to 20% of polyisocyanate, 3 to 15% of methylene succinic acid, 1 to 8% of polyether urethane, 1 to 5% of isophorone diamine, 2 to 10% of glycidyl methacrylate, 5 to 15% of acrylate, 3 to 10% of styrene, 0 to 8% of isopropanol and 1 to 5% of an auxiliary agent, with the balance being deionized water. The invention also discloses a preparation method for the above-mentioned waterborne aromatic polyisocyanate cross-linking agent. Compared with the prior art, the preparation method provided by the invention has the following advantages: the synthetic process is simple and standardized; the production process and production flow are easy to control; meanwhile, a product prepared by using the preparation method provided by the invention has reliable performance and good stability; production experience can be conveniently summarized and accumulated; production raw materials have good environmental protection performance; meanwhile, the waterborne aromatic polyisocyanate cross-linking agent provided by the invention effectively improves reaction efficiency of the raw materials and controlling and adjusting abilities to the reaction process, and has the characteristics of strong adhesion force, high peel strength, proper softness, good water resistance and scrubbing resistance and low film-forming temperature.

Description

technical field [0001] The invention belongs to the technical field of new materials, and particularly relates to a water-based aromatic polyisocyanate crosslinking agent and a preparation method thereof. Background technique [0002] Polyisocyanate crosslinking agent is a very frequently used raw material in the textile industry, which has an extremely important impact on the production, processing and performance of textiles. However, in actual use, it is found that the currently used polyisocyanate crosslinking agent The traditional formulas and processes that are often used in the agent can meet the needs of use to a certain extent, but its own toxicity is relatively large, and it is more harmful to the surrounding environment and users. At the same time, there are also insufficient adhesion and softness. , water resistance and low scrub resistance, so it cannot effectively meet the needs of actual use, and the product quality stability of related products is relatively ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L75/00C08L75/08C08L71/02C08K5/00C08K5/17C08K5/092C08K5/053C08K5/526
CPCC08L75/00C08L2205/035C08L75/08C08L71/02C08K5/00C08K5/17C08K5/092C08K5/053C08K5/526
Inventor 沈健赵刚
Owner 上海浩登材料股份有限公司
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