Anti-oxidation coating for nuclear fuel pellets and preparation method thereof
A nuclear fuel and anti-oxidation technology, applied in the direction of uranium dioxide, reactor fuel material, uranium oxide/hydroxide, etc., to achieve the effect of preventing oxidation
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Embodiment 1
[0024] Embodiment 1: Preparation of nuclear fuel pellet anti-oxidation coating (1)
[0025] UO was prepared by the following steps 2 Antioxidant coatings for nuclear fuel pellets.
[0026] (1) Preparation of polycarbosilane solution
[0027] Take 10g of polycarbosilane (provided by National University of Defense Technology, molecular weight 1400-2000) and dissolve it in 100ml of petroleum ether. During the dissolution process, if necessary, heat it in a water bath to 40°C and stir. After the dissolution is complete, cool to room temperature and filter to obtain a polycarbosilane solution.
[0028] (2) Coating of polycarbosilane protective layer
[0029] The polycarbosilane solution was transferred to an argon-protected glove box, and the UO 2 The pellet is immersed in the polycarbosilane solution, taken out to dry, and repeated 4 times to complete the preparation of the polycarbosilane coating.
[0030] The anti-oxidation coating thus prepared has a thickness of 10-20 μm....
Embodiment 2
[0031] Embodiment 2: Preparation of nuclear fuel pellet anti-oxidation coating (two)
[0032] Utilize the method for following steps to prepare substoichiometric uranium dioxide (UO 2-x ) anti-oxidation coating of nuclear fuel pellets.
[0033] (1) Preparation of polycarbosilane solution
[0034] Take 30g of polycarbosilane (provided by National University of Defense Technology, molecular weight 1400-2000) and dissolve it in 100ml of cyclohexane. During the dissolution process, if necessary, heat it to 60°C in a water bath and stir. After the dissolution is complete, cool to room temperature and filter to obtain a polycarbosilane solution.
[0035] (2) Coating of polycarbosilane protective layer
[0036] The polycarbosilane solution was transferred to an argon-protected glove box, and substoichiometric uranium dioxide (UO 2-x ) The pellet is immersed in the polycarbosilane solution, taken out to dry, and repeated 3 times to complete the preparation of the polycarbosilane c...
Embodiment 3
[0038] Embodiment 3: Preparation of nuclear fuel pellet anti-oxidation coating (three)
[0039] The anti-oxidation coating of the MOX nuclear fuel pellets is prepared by the following steps.
[0040] (1) Preparation of polycarbosilane solution
[0041] Take 20g polycarbosilane (provided by National University of Defense Technology, molecular weight 1400-2000) and dissolve it in 100ml xylene. During the dissolution process, if necessary, heat it to 50°C in a water bath and stir. After the dissolution is complete, cool to room temperature and filter to obtain a polycarbosilane solution.
[0042] (2) Coating of polycarbosilane protective layer
[0043] Transfer the polycarbosilane solution to an argon-protected glove box, immerse the MOX pellet in the polycarbosilane solution, take it out to dry, and repeat 4 times to complete the preparation of the polycarbosilane coating.
[0044] The anti-oxidation coating thus prepared has a thickness of 40-60 μm.
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