The invention belongs to the technical field of
product analysis and inspection, and particularly relates to a
metallography detection method of MOX
pellets.
MOX fuel pellets with intact surfaces andno cracks are selected, and
sodium sulfide is added into
epoxy resin to configure an inlay sample agent; the
MOX fuel pellets are placed in the central position of phenolic resin inlay sample sleeves,the inlay sample agent is poured in, and after standing and solidification of the inlay sample agent, inlaid samples are taken from the inlay sample sleeves; the inlaid samples are arranged in clamping plates of a
grinding and
polishing device and fixed,
grinding is conducted on
grinding and
polishing plates from coarse to fine separately, and
sample water is washed each time when the grinding and
polishing plates are replaced; the washed samples continue to be arranged in the grinding plates and fixed, and the samples are polished on a lint, meanwhile the Al2O3 grinding and polishing liquidis poured on the grinding and polishing plates, and the samples are washed with water after the grinding and polishing;
corrosion soaking is conducted on the ground and polished samples using a
corrosion liquid prepared from HNO3 and HCl, and then the surfaces of the samples are washed with water after the
corrosion soaking, and rinsing and dry blowing are conducted using
anhydrous ethanol. According to the
metallography detection method of the MOX pellets, accurate measurements of the grain sizes of the pellets and equivalent diameters of pores can be achieved.