The invention belongs to the technical field of 
product analysis and inspection, and particularly relates to a 
metallography detection method of MOX 
pellets. 
MOX fuel pellets with intact surfaces andno cracks are selected, and 
sodium sulfide is added into 
epoxy resin to configure an inlay sample agent; the 
MOX fuel pellets are placed in the central position of phenolic resin inlay sample sleeves,the inlay sample agent is poured in, and after standing and solidification of the inlay sample agent, inlaid samples are taken from the inlay sample sleeves; the inlaid samples are arranged in clamping plates of a 
grinding and 
polishing device and fixed, 
grinding is conducted on 
grinding and 
polishing plates from coarse to fine separately, and 
sample water is washed each time when the grinding and 
polishing plates are replaced; the washed samples continue to be arranged in the grinding plates and fixed, and the samples are polished on a lint, meanwhile the Al2O3 grinding and polishing liquidis poured on the grinding and polishing plates, and the samples are washed with water after the grinding and polishing; 
corrosion soaking is conducted on the ground and polished samples using a 
corrosion liquid prepared from HNO3 and HCl, and then the surfaces of the samples are washed with water after the 
corrosion soaking, and rinsing and dry blowing are conducted using 
anhydrous ethanol. According to the 
metallography detection method of the MOX pellets, accurate measurements of the grain sizes of the pellets and equivalent diameters of pores can be achieved.