Textile printing and dyeing fixer and preparation method thereof

A color-fixing agent and textile technology, applied in dyeing, textiles and papermaking, etc., can solve the problems of low wet rubbing fastness and low utilization rate of dyed fabrics, and improve dry rubbing fastness and quality , High color fastness effect

Inactive Publication Date: 2018-11-16
陈国宝
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in the printing and dyeing process, the utilization rate is relatively low, and the wet rubbing fastness of the dyed fabric, especially the wet rubbing fastness of the medium and dark fabrics is low, so the fabric needs to be fixed with a color-fixing agent after the dyeing process. treated to improve its color fastness

Method used

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  • Textile printing and dyeing fixer and preparation method thereof
  • Textile printing and dyeing fixer and preparation method thereof
  • Textile printing and dyeing fixer and preparation method thereof

Examples

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Effect test

preparation example Construction

[0027] A kind of preparation method of textile printing and dyeing fixing agent of the present invention, realizes by following steps:

[0028] (1) Put the cationic monomer, 1,3-diallylamino-2-hydroxypropane, (meth)acrylate monomer containing isocyanate group and water into the polymerization reaction vessel, stir evenly, and heat heat up;

[0029] (2) Under anaerobic conditions and stirring conditions, drip initiator solution in the polymerization reaction vessel, carry out polymerization reaction, the temperature of polymerization reaction is 80~100 ℃, and the mass concentration of initiator solution is 1~10%, here The initiator solution is prepared from the initiator and part of the water, and the initiator solution is dripped within 1 to 3 hours;

[0030] (3) After the dropwise addition is completed, continue to carry out the polymerization reaction at the temperature of the polymerization reaction for 1 to 3 hours, then cool down to room temperature and discharge to obta...

Embodiment 1

[0033] A kind of textile printing and dyeing fixing agent of the present invention is made of the following raw material components with the ratio of parts by mass:

[0034]

[0035] A kind of preparation method of textile printing and dyeing fixing agent of the present invention, realizes by following steps:

[0036] (1) Put 26 parts of diallyltrimethylammonium chloride, 1.5 parts of 1,3-diallylamino-2-hydroxypropane, 2 parts of 2-isocyanate ethyl acrylate, and 65.4 parts of water into In the polymerization reaction vessel, stir evenly, and heat up;

[0037] (2) Under anaerobic conditions and stirring conditions, add ammonium persulfate solution dropwise to the polymerization reaction vessel to carry out polymerization reaction. The temperature of the polymerization reaction is 82 ° C, and the mass concentration of ammonium persulfate solution is 2%. The ammonium solution is prepared from 0.1 part of ammonium persulfate and 4.9 parts of water, and the dropping time is con...

Embodiment 2

[0040] A kind of textile printing and dyeing fixing agent of the present invention is made of the following raw material components with the ratio of parts by mass:

[0041]

[0042] A kind of preparation method of textile printing and dyeing fixing agent of the present invention, realizes by following steps:

[0043] (1) Put 28 parts of methyl diallyl ammonium chloride, 3 parts of 1,3-diallylamino-2-hydroxypropane, 2.5 parts of 2-isocyanate ethyl methacrylate, and 56.5 parts of water into Into the polymerization reaction vessel, stir evenly, and heat up;

[0044] (2) Under anaerobic conditions and stirring conditions, add ammonium persulfate solution dropwise to the polymerization reaction vessel to carry out polymerization reaction. The temperature of the polymerization reaction is 86 ° C, and the mass concentration of ammonium persulfate solution is 3%. The ammonium solution is prepared from 0.3 parts of ammonium persulfate and 9.7 parts of water, and the dropping time ...

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Abstract

The invention provides a textile printing and dyeing fixer and a preparation method thereof. The preparation method comprises the following steps: (1) putting a cationic monomer, 1,3-diallylamino-2-hydroxypropane, a (methyl)acrylate monomer containing an isocyanate group and water into a polymerization reaction vessel, uniformly stirring, heating and warming; (2) in a condition without oxygen anda condition of stirring, dropwise adding initiator solution to the polymerization reaction vessel, performing a polymerization reaction, wherein a temperature of the polymerization reaction is 80-100DEG C, and a mass concentration of the initiator solution is 1-10%, so the initiator solution is prepared by an initiator and a part of the water, and completely dropwise adding the initiator solutionwithin 1-3 hours; and (3) after completely dropwise adding, in the temperature of the polymerization reaction, continuously performing the polymerization reaction for 1-3 hours, cooling to room temperature, and discharging, to obtain the fixer.

Description

technical field [0001] The invention belongs to the technical field of textile auxiliaries, in particular to a textile printing and dyeing color fixing agent and a preparation method thereof. Background technique [0002] Cotton fabric fiber has become one of the most popular fabric fibers due to its superior wearing performance and environmental protection. It is widely used because of its good hygroscopicity, warmth retention, comfort and soft feel, as well as the characteristics of cleaning, health care, degradable recycling and so on. At present, the dyes used in cotton fiber printing and dyeing include vat dyes, sulfur dyes, direct dyes and reactive dyes. [0003] Reactive dyes, as the focus of development and use in cotton fabric dyes, have many advantages such as complete color spectrum, bright color, low price and convenient use. However, in the printing and dyeing process, the utilization rate is relatively low, and the wet rubbing fastness of the dyed fabric, esp...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P5/08D06P1/38D06P3/66C08F226/02C08F220/34
CPCC08F226/02D06P1/38D06P3/66D06P5/08C08F220/34
Inventor 陈国宝
Owner 陈国宝
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