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Environmentally friendly acrylic resin and preparation method thereof

An acrylic resin and an environment-friendly technology, applied in the field of environment-friendly acrylic resin and its preparation and processing of nail polish, can solve the problems of low solid content of nail polish, toxicity to the human body and the environment, etc., and achieve good hardness, good hydrophobicity, organic The effect of less solvent

Active Publication Date: 2018-12-07
莱阳红安化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] From the above formula, the existing nail polish has a low solid content, and the resin contains benzene solvents and formaldehyde, which are harmful to the human body and the environment.

Method used

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  • Environmentally friendly acrylic resin and preparation method thereof
  • Environmentally friendly acrylic resin and preparation method thereof
  • Environmentally friendly acrylic resin and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0052] A kind of environment-friendly acrylic resin of the present embodiment comprises following raw material:

[0053] Bottom material: 3 grams of E10P material, 3 grams of amyl acetate, 13 grams of n-butyl acetate

[0054] Mixed dripping material: 1.5 grams of methacrylic acid, 5 grams of methyl methacrylate, 16 grams of styrene, 5.5 grams of tert-butyl acrylate, 3.5 grams of hydroxyethyl methacrylate, 5.5 grams of 2-hydroxypropyl acrylate, methyl 2 g of n-butyl acrylate, 4 g of n-butyl acrylate, 1.8 g of dicumyl peroxide, 0.8 g of 1,1-bis(tert-butylperoxy)cyclohexane, and 1 g of n-butyl acetate;

[0055] Initiator 1: 0.10 g of 1,1-bis(tert-butylperoxy)cyclohexane, 1 g of n-butyl acetate;

[0056] Initiator 2: 0.10 g of 1,1-bis(tert-butylperoxy)cyclohexane, 1 g of n-butyl acetate;

[0057] Diluent: 2 grams of n-butyl acetate;

[0058] A preparation method of environment-friendly acrylic resin, comprising the following steps:

[0059] 1. Add 3 grams of E10P material, 3 g...

Embodiment 2

[0065] A kind of environment-friendly acrylic resin of the present embodiment comprises following raw material:

[0066] Bottom material: 4.5 grams of E10P material, 4 grams of amyl acetate, 17 grams of n-butyl acetate

[0067] Mixed dripping material: 2.3 grams of methacrylic acid, 7.5 grams of methyl methacrylate, 21 grams of styrene, 7.5 grams of tert-butyl acrylate, 5 grams of hydroxyethyl methacrylate, 8.5 grams of 2-hydroxypropyl acrylate, methyl 3 g of n-butyl acrylate, 6 g of n-butyl acrylate, 2.0 g of dicumyl peroxide, 1.0 g of 1,1-bis(tert-butyl peroxy)cyclohexane, and 1 g of n-butyl acetate;

[0068] Initiator 1: 0.15 g of 1,1-bis(tert-butylperoxy)cyclohexane, 1.5 g of n-butyl acetate;

[0069] Initiator 2: 0.15 g of 1,1-bis(tert-butylperoxy)cyclohexane, 1.5 g of n-butyl acetate;

[0070] Diluent: 3 grams of n-butyl acetate;

[0071] A preparation method of environment-friendly acrylic resin, comprising the following steps:

[0072] 1. Add 4.5 grams of E10P mate...

Embodiment 3

[0078] A kind of environment-friendly acrylic resin of the present embodiment comprises following raw material:

[0079] Bottom material: 6.0 grams of E10P material, 5 grams of amyl acetate, 20 grams of n-butyl acetate

[0080] Mixed dripping material: 3 grams of methacrylic acid, 10 grams of methyl methacrylate, 25 grams of styrene, 9.5 grams of tert-butyl acrylate, 6.0 grams of hydroxyethyl methacrylate, 9.5 grams of 2-hydroxypropyl acrylate, methyl 4.0 g of n-butyl acrylate, 7.0 g of n-butyl acrylate, 2.2 g of dicumyl peroxide, 1.1 g of 1,1-bis(tert-butyl peroxy)cyclohexane, and 1 g of n-butyl acetate;

[0081] Initiator 1: 0.2 g of 1,1-bis(tert-butylperoxy)cyclohexane, 2.0 g of n-butyl acetate;

[0082] Initiator 2: 0.2 g of 1,1-bis(tert-butylperoxy)cyclohexane, 2.0 g of n-butyl acetate;

[0083] Diluent: 4 grams of n-butyl acetate;

[0084] A preparation method of environment-friendly acrylic resin, comprising the following steps:

[0085] 1. Add 6.0 grams of E10P mat...

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Abstract

The invention relates to an environmentally friendly acrylic resin and a preparation method thereof, especially suitable for processing nail polish, and belongs to the technical field of polymer materials. The raw materials of the acrylic resin include, by weight, a kettle bed material, a mixed dropping material, an initiator 1, an initiator 2 and a diluent; the kettle bed material includes E10P,amyl acetate and n-butyl acetate; the mixed dropping material includes methacrylic acid, methyl methacrylate, styrene, tert-butyl acrylate, hydroxyethyl methacrylate, 2-hydroxypropyl acrylate, butyl methacrylate, butyl acrylate, dicumyl peroxide, 1,1-di(tert-butylperoxy)cyclohexane and the n-butyl acetate; the initiator 1 includes the 1,1-di(tert-butylperoxy)cyclohexane and the n-butyl acetate; the initiator 2 includes the 1,1-di(tert-butylperoxy)cyclohexane and the n-butyl acetate; and the diluent includes the n-butyl acetate. The acrylic resin is high in environmental protection, so that theexistence of substances harmful to human bodies can be completely solved, and the use amount of solvents can be greatly reduced.

Description

technical field [0001] The invention relates to an environment-friendly acrylic resin and a preparation method thereof, which is especially suitable for processing nail polish and belongs to the technical field of polymer materials. Background technique [0002] Nail polish is a cosmetic widely used on fingernails or toenails. It is rich in color and has both aesthetic and protective effects. The composition of nail polish is generally composed of two types of substances, one is solid components, mainly pigments, flash substances, etc., and the other is liquid components, and liquid components can be divided into two types, one is solvent components, the other The first is a polymer solution, that is, a film former resin, which contains nitrocellulose and synthetic resin to increase quick drying. Synthetic resins used for nail polish mainly refer to hydroxyl-containing saturated polyesters and hydroxyl-containing acrylic resins, because these resins are compatible with nitr...

Claims

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Application Information

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IPC IPC(8): C08F212/08C08F220/06C08F220/14C08F220/18C08F220/20A61K8/81A61Q3/02
CPCA61K8/8147A61Q3/02C08F212/08C08F220/06C08F220/14C08F220/1804C08F220/20
Inventor 安华钟学海高健荣宋吉春林永辉车彦仪李季
Owner 莱阳红安化工有限公司
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