Composite fiber, and application thereof in insect-proof net for rice
A composite fiber and insect-proof net technology, which is applied in the field of fiber and its application, can solve the problems of affecting the use effect, uneven distribution of rare earth ions, and the inability of the insect-proof net to completely eliminate the main pests, so as to improve the strength, increase the yield, and increase the insect-proof effect Effect
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[0030] 1.1 Preparation of chitosan particles
[0031] Sample 1:
[0032] Step 1: dissolving chitosan with an average molecular weight of 20000KDa in the acetic acid solution of 1mol / L, adding copper stearate and europium chloride for dissolution, the mass ratio of chitosan, copper stearate and europium ions is 1: 0.1:0.02.
[0033] Step 2: Add 0.1 mol / L sodium hydroxide solution dropwise to the mixed solution, so that the pH of the solution is 6.0-8.0.
[0034] Step 3: Concentrate the obtained solution and freeze-dry to obtain chitosan particles.
[0035] Sample 2:
[0036] Step 1: dissolving chitosan with an average molecular weight of 20000KDa in the acetic acid solution of 1mol / L, adding copper stearate and europium chloride for dissolution, the mass ratio of chitosan, copper stearate and europium ions is 2: 0.5:0.05.
[0037] Step 2: Add 0.1 mol / L sodium hydroxide solution dropwise to the mixed solution, so that the pH of the solution is 6.0-8.0.
[0038] Step 3: Con...
Embodiment 1
[0057]Embodiment 1: use the N, N-dimethylformamide and chloroform mixed solvent that volume ratio is 50:50, prepare 10wt% polyurethane solution, the chitosan microparticle of prepared sample 1, the sample prepared in 1.2 part Add the emulsion granule of 4 into the polyurethane solution and stir, mix evenly and then add the solution into the syringe and electrospin to obtain a composite fiber, the chitosan particle weight percentage in the composite fiber is 1wt%, and the emulsion particle in the composite fiber The weight percentage of agent is 0.1wt%.
Embodiment 2
[0058] Embodiment 2: use the N, N-dimethylformamide and chloroform mixed solvent that volume ratio is 50:50, prepare 10wt% polyurethane solution, the chitosan microparticle of prepared sample 2, the sample prepared in 1.2 part Add the emulsion granule of 4 into the polyurethane solution and stir, mix evenly and then add the solution into the syringe and electrospin to obtain a composite fiber, the chitosan particle weight percentage in the composite fiber is 5wt%, the emulsion in the composite fiber The agent weight percentage is 3wt%.
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