Preparation method and application of a freshness-indicating smart label
A smart label and freshness technology, which is applied in the field of food packaging storage and detection, can solve the problems of large amount of indicator, weak fixation, high production cost, etc., achieve convenience and intuitiveness, improve fixation firmness and response sensitivity, and quickly identify food the quality of the effect
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Embodiment 1
[0023] A preparation method of a freshness indicating smart label is as follows:
[0024] (1) Label substrate pretreatment:
[0025] Use low-temperature plasma to pretreat the surface of polycaprolactone (PCL) film as the label substrate. The low-temperature plasma treatment process conditions are: the ratio of air flow to oxygen flow is 2:1, and the air flow is 0.5L / min ;The current is set to 0.8A, the voltage is 150V; the vacuum is 1600Pa; the processing time is 1min;
[0026] (2) Preparation of nanocellulose film-forming solution containing color developer:
[0027] Anthocyanin natural pigment powder is dissolved in ethanol solution with a volume concentration of 70%, and magnetically stirred at room temperature for 1 hour to prepare a pigment solution with a pigment concentration of 3%; it is prepared by mechanical grinding method using bleached hardwood fiber as raw material Nanocellulose with a diameter of 2 to 20 nm and a length of 0.1 to 100 μm. Use distilled water ...
Embodiment 2
[0032] A preparation method of a freshness indicating smart label is as follows:
[0033] (1) Label substrate pretreatment:
[0034] Use low-temperature plasma to pretreat the surface of the polylactic acid (PLA) film as the label substrate. The low-temperature plasma treatment process conditions are: the ratio of air flow to oxygen flow is 1:1, and the air flow is 0.1L / min; The setting is 0.5A, the voltage is 100V; the vacuum is 500Pa; the processing time is 5min;
[0035] (2) Preparation of nanocellulose film-forming solution containing color developer:
[0036] Dissolve fungal-fermented natural pigment powder in an ethanol solution with a volume concentration of 70%, and magnetically stir it at room temperature for 1 hour to prepare a pigment solution with a pigment concentration of 3%. The bleached bagasse fiber is used as a raw material to prepare a diameter of 2 ~20nm nanocellulose with a length of 0.1~100μm. Use distilled water to disperse nanocellulose into a suspen...
Embodiment 3
[0041] A preparation method of a freshness indicating smart label is as follows:
[0042] (1) Label substrate pretreatment:
[0043] Use low-temperature plasma to pretreat the surface of the polylactic acid (PLA) film as the label substrate. The low-temperature plasma treatment process conditions are: the ratio of air flow to oxygen flow is 3:1, and the air flow is 0.9L / min; current The setting is 0.3A, the voltage is 200V; the vacuum is 1000Pa; the processing time is 3min;
[0044] (2) Preparation of nanocellulose film-forming solution containing color developer:
[0045] Mix methyl red powder and bromothymol blue powder according to a mass ratio of 3:2, dissolve in an ethanol solution with a volume concentration of 70%, stir magnetically at room temperature for 1 hour, and prepare a pigment solution with a pigment concentration of 3%; The nano-cellulose with a diameter of 2-20 nm and a length of 0.1-100 μm is prepared by using the bleached coniferous wood fiber as a raw mate...
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