Filter assembly, method for manufacturing same, and filter module comprising same
A manufacturing method and filter technology, applied in membrane filters, chemical instruments and methods, separation methods, etc., can solve the problems of inability to ensure flow paths, damaged separation membranes, low durability, etc., and achieve excellent water permeability and durability. The effect of improving the hydrophilicity, prolonging the service life and improving the hydrophilicity
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Embodiment 1
[0117] First, to prepare a spinning solution, in 88 g of a mixed solvent of dimethylacetamide and acetone at a weight ratio of 70:30, 12 g of polyfluorescein, which is a fiber-forming component, was melted at a temperature of 80°C using a magnetic bar. Ethylene difluoride (Arkema, Kynar 761) was dissolved for 6 hours to prepare a mixed solution. The above-mentioned spinning solution was put into the solution tank of the electrospinning device, and discharged at a rate of 15 μl / min / hole. At this time, the temperature in the spinning zone was kept at 30° C., the humidity was kept at 50%, and the distance between the collector and the tip of the spinning nozzle was 20 cm. Then, a voltage of more than 40kV was applied to the spinning nozzle assembly (SpinNozzle Pack) using a high voltage generator, and an air pressure of 0.03MPa was applied to each spinning assembly nozzle to prepare a fiber web layer formed by PVDF nanofibers. Then, in order to dry the solvent and moisture remai...
Embodiment 2~ Embodiment 18
[0124] Except changing the component etc. of hydrophilic coating composition as shown in following table 1, table 2 or table 3, all the other make the filter shown in following table 1, table 2 or table 3 in the same way as embodiment 1 aggregate.
experiment example 1
[0128] In the manufacturing process of the filter assembly according to the Examples and Comparative Examples, the following physical properties of the fiber web formed with the hydrophilic coating layer manufactured before bonding with the second support were evaluated, and the results are shown in Table 1 to Table 1. 3.
[0129] 1. Measuring the wetting angle
[0130]A contact angle (Contact angle, °) measuring device is used to measure the contact angle formed by the surface of the fiber web layer and the surface of the water drop to measure the wettability (wettability) of water on the exposed surface of the fiber web layer. A method of photographing the shape of a droplet with a CCD camera and calculating the interfacial tension γ optimized for the last photographed droplet shape was used. Adjust the injection volume to 0.05 mL via a microsyringe and use double distilled water. The contact angle was measured within 20 seconds after the droplet was formed at five points ...
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