Tobacco flue-cured fragrant cigarette pop bead capable of reducing smoke free radicals and preparation method thereof
A technology of free radicals and tobacco, which is applied in the direction of tobacco, application, smoke oil filter, etc., can solve the problems of not prominent roasting aroma, increase cigarette irritation and miscellaneous gas, etc., and achieve improvement of roasting aroma and smoking taste , Improving the quality of baking aroma and the effect of product safety
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Embodiment 1
[0032] In terms of parts by weight, 10 parts of Zimbabwe flue-cured tobacco, 1 part of Greek oriental tobacco, 5 parts of Sichuan sun-cured red tobacco, 100 parts of ethylene glycol, 0.01 part of ferric chloride-ethylenediaminetetraacetic acid compound (mol Ratio 1:3) into a round-bottomed flask, stirred, connected to the mouth of the flask to reflux, then placed in an oil bath and heated to 150°C, and reacted for 3 hours. Add 200 parts of petroleum ether to the above reaction product, ultrasonically extract for 60 minutes, then shake and extract for 60 minutes, then carry out centrifugation for 15 minutes, take the upper layer liquid and filter it with an organic filter membrane, carry out vacuum distillation, and remove the solvent to obtain the desired concentrate.
[0033] Dissolve 5 parts by weight of the above-mentioned concentrate in water to form a 5% solution, then add 2.5 parts by weight of baicalin, stir at room temperature for 20 minutes to dissolve the ingredients...
Embodiment 2
[0038] According to parts by weight, each 30 parts of Henan flue-cured tobacco and Yunnan flue-cured tobacco, 2 parts of Turkish oriental tobacco and 3 parts of Xinjiang oriental tobacco, tobacco powder of 25 parts each of Hunan sun-cured red tobacco and Guangdong sun-cured red tobacco, 250 parts of propylene glycol, and zinc lactate - Add 1 part of the tartaric acid compound (molar ratio 1:5) into a round-bottomed flask, stir, connect a condenser to the mouth of the flask to reflux, then put it into an oil bath and heat to 250°C, and react for 0.5h. Add 2000 parts of n-hexane and chloroform to the above reaction product, ultrasonically extract for 10 minutes, then shake and extract for 10 minutes, then centrifuge for 4 minutes, take the upper liquid and filter it with an organic filter membrane, carry out vacuum distillation, and remove the solvent to obtain the obtained product. Concentrate required.
[0039] Dissolve 15 parts by weight of the above concentrate in caprylic c...
Embodiment 3
[0043]According to parts by weight, 30 parts of American flue-cured tobacco, 2 parts of Baoshan oriental tobacco, 18 parts of Jilin sun-cured red tobacco, 200 parts of glycerin, and 0.1 part of zinc lactate-tartaric acid compound (molar ratio 1:5) were added to the circle. Bottom flask, stirred, the mouth of the flask was connected with a condenser to reflux, then placed in an oil bath and heated to 200°C, and reacted for 1 hour. Add 1000 parts of ethyl acetate to the above reaction product, ultrasonically extract for 30 minutes, then shake and extract for 30 minutes, then centrifuge for 4 minutes, take the upper liquid and filter it with an organic filter membrane, then carry out vacuum distillation to remove the solvent, and obtain the desired product. concentrates.
[0044] Dissolve 10 parts by weight of the above-mentioned concentrate in caprylic capric acid glyceride to form a 10% solution, then add 8 parts by weight of baicalin, stir at room temperature for 25 minutes un...
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