Tobacco flue-cured fragrant cigarette pop bead capable of reducing smoke free radicals and preparation method thereof

A technology of free radicals and tobacco, which is applied in the direction of tobacco, application, smoke oil filter, etc., can solve the problems of not prominent roasting aroma, increase cigarette irritation and miscellaneous gas, etc., and achieve improvement of roasting aroma and smoking taste , Improving the quality of baking aroma and the effect of product safety

Active Publication Date: 2019-01-25
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the roasted fragrance of the above-mentioned products obtained is not outstanding, and still contains a certain amount of macromolecular substances such as protein, pectin, and polysaccharides, which will be cracked to produce some harmful components during the smoking process of cigarettes, which will increase the quality of cigarettes. Suction irritation and fumes

Method used

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  • Tobacco flue-cured fragrant cigarette pop bead capable of reducing smoke free radicals and preparation method thereof
  • Tobacco flue-cured fragrant cigarette pop bead capable of reducing smoke free radicals and preparation method thereof
  • Tobacco flue-cured fragrant cigarette pop bead capable of reducing smoke free radicals and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] In terms of parts by weight, 10 parts of Zimbabwe flue-cured tobacco, 1 part of Greek oriental tobacco, 5 parts of Sichuan sun-cured red tobacco, 100 parts of ethylene glycol, 0.01 part of ferric chloride-ethylenediaminetetraacetic acid compound (mol Ratio 1:3) into a round-bottomed flask, stirred, connected to the mouth of the flask to reflux, then placed in an oil bath and heated to 150°C, and reacted for 3 hours. Add 200 parts of petroleum ether to the above reaction product, ultrasonically extract for 60 minutes, then shake and extract for 60 minutes, then carry out centrifugation for 15 minutes, take the upper layer liquid and filter it with an organic filter membrane, carry out vacuum distillation, and remove the solvent to obtain the desired concentrate.

[0033] Dissolve 5 parts by weight of the above-mentioned concentrate in water to form a 5% solution, then add 2.5 parts by weight of baicalin, stir at room temperature for 20 minutes to dissolve the ingredients...

Embodiment 2

[0038] According to parts by weight, each 30 parts of Henan flue-cured tobacco and Yunnan flue-cured tobacco, 2 parts of Turkish oriental tobacco and 3 parts of Xinjiang oriental tobacco, tobacco powder of 25 parts each of Hunan sun-cured red tobacco and Guangdong sun-cured red tobacco, 250 parts of propylene glycol, and zinc lactate - Add 1 part of the tartaric acid compound (molar ratio 1:5) into a round-bottomed flask, stir, connect a condenser to the mouth of the flask to reflux, then put it into an oil bath and heat to 250°C, and react for 0.5h. Add 2000 parts of n-hexane and chloroform to the above reaction product, ultrasonically extract for 10 minutes, then shake and extract for 10 minutes, then centrifuge for 4 minutes, take the upper liquid and filter it with an organic filter membrane, carry out vacuum distillation, and remove the solvent to obtain the obtained product. Concentrate required.

[0039] Dissolve 15 parts by weight of the above concentrate in caprylic c...

Embodiment 3

[0043]According to parts by weight, 30 parts of American flue-cured tobacco, 2 parts of Baoshan oriental tobacco, 18 parts of Jilin sun-cured red tobacco, 200 parts of glycerin, and 0.1 part of zinc lactate-tartaric acid compound (molar ratio 1:5) were added to the circle. Bottom flask, stirred, the mouth of the flask was connected with a condenser to reflux, then placed in an oil bath and heated to 200°C, and reacted for 1 hour. Add 1000 parts of ethyl acetate to the above reaction product, ultrasonically extract for 30 minutes, then shake and extract for 30 minutes, then centrifuge for 4 minutes, take the upper liquid and filter it with an organic filter membrane, then carry out vacuum distillation to remove the solvent, and obtain the desired product. concentrates.

[0044] Dissolve 10 parts by weight of the above-mentioned concentrate in caprylic capric acid glyceride to form a 10% solution, then add 8 parts by weight of baicalin, stir at room temperature for 25 minutes un...

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Abstract

The invention relates to tobacco flue-cured fragrant cigarette pop beads capable of reducing smoke free radicals and a preparation method thereof, belonging to the technical field of cigarette auxiliary materials. The method comprises adding a polyol and an organic acid- metal salt compound to tobacco powder to be uniformly mixed and reacted at 150-250 DEG C for 0.5-3h, the obtained product is added into an organic solvent, ultrasonic extraction is carried out first, then vibration extraction is carried out, centrifugal separation is carried out, the upper liquid is filtered by an organic filter membrane, and the filtrate is distilled under reduced pressure to obtain a concentrate; 5 to 15 percents of concentrate is prepared into solution by using water or glyceryl octyl decanoate as solvent, then baicalin is added into that solution, uniformly stirred at room temperature, then the solution is put in a shade place to be alcoholized, and finally, the alcoholic solution is taken as corematerial, and is made into drop pills by use a dripping pill machine, and dried to obtain the dripping pills. The preparation method is simple, the cost is low, the cigarette pop bead prepared by theinvention can remarkably reduce the free radical content in the smoke, and has a good application prospect.

Description

technical field [0001] The invention belongs to the technical field of auxiliary materials for tobacco, and in particular relates to popping beads for tobacco-flavored tobacco that can reduce smoke free radicals and a preparation method thereof. Background technique [0002] As cigarette consumers pay more and more attention to their own health and have higher and higher requirements for the inherent quality of cigarettes, low-tar and high-quality cigarettes have become the focus of current tobacco research. However, low tar must be accompanied by loss of cigarette aroma and poor comfort. In terms of quality, the current domestic cigarette products have certain deficiencies in smoking quality and sensory comfort, such as weak aroma, strong dryness, insufficient sweetness, and poor comfort. [0003] Popping bead cigarettes are pre-embedded with one or more flavor capsules in the puffing beads for cigarettes, and the smoker can selectively pinch and pop the capsules during th...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24D3/06
CPCA24D3/061
Inventor 孔维松张承明王晋刘强侯春陈建华耿永勤魏玉玲田丽梅张涛杨光宇
Owner CHINA TOBACCO YUNNAN IND
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