Ni@LaCO3OH composite material as well as preparation method and application thereof
A composite material, CO2 technology, applied in the field of composite materials, can solve the problems of small volume, high energy density, etc., achieve high catalytic efficiency, long catalytic life, and protect the environment
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0041] (1) In a glove box with an argon atmosphere of 0.1MPa, take 4.5g of LaNi that has been arc-melted and fully crushed, and screened through a 200-mesh standard inspection sieve. 5 Put the powder into a 25mL high-temperature and high-pressure reactor (NS-25-316L), fill it with 4MPa hydrogen, place it at 150°C for 5 hours to fully activate it, and cool to room temperature;
[0042] (2) Pump out the remaining gas in the kettle (the pressure in the kettle is between 0.1 and 1MPa during the pumping process), and fill it with a mixed gas containing 3MPa carbon dioxide (V CO2 :V Ar =19:81), pumping and inflating again, after repeating 5 times, there is no hydrogen residue in the reactor, and the mixed gas containing carbon dioxide of 3MPa (V CO2 :V Ar =19:81), the reactor was placed at 180°C for reaction, after 40 hours of reaction, the reactor was cooled to room temperature, and the Ni@LaCO 3 OH composite material;
[0043] (3) Take out all the remaining gas in the kettle, ...
Embodiment 2
[0045] (1) In a glove box with an argon atmosphere of 0.1MPa, take 4.5g of LaNi that has been arc-melted and fully crushed, and screened through a 200-mesh standard inspection sieve. 5 Put the powder into a 25mL high-temperature and high-pressure reactor (NS-25-316L), fill it with 4MPa hydrogen, place it at 150°C for 5 hours to fully activate it, and cool to room temperature;
[0046] (2) Pump out the remaining gas in the kettle (the pressure in the kettle is between 0.1 and 1MPa during the pumping process), and fill it with a 3MPa mixed gas containing carbon dioxide (V CO2 :V Ar =19:81), pumping and inflating again, after repeating 5 times, there is no hydrogen residue in the reactor, and the mixed gas containing carbon dioxide of 3MPa (V CO2 :V Ar =19:81), the reactor was placed at 180°C for reaction, after 40 hours of reaction, the reactor was cooled to room temperature, and the Ni@LaCO 3 OH composite material;
[0047] (3) Take out all the remaining gas in the kettle, ...
Embodiment 3
[0051] (1) In a glove box with an argon atmosphere of 0.1MPa, take 4.5g of LaNi that has been arc-melted and fully crushed, and screened through a 200-mesh standard inspection sieve. 5 Put the powder into a 25mL high-temperature and high-pressure reactor (NS-25-316L), fill it with 4MPa hydrogen, place it at 150°C for 5 hours to fully activate it, and cool to room temperature;
[0052] (2) Pump out the remaining gas in the kettle (the pressure in the kettle is between 0.1 and 1MPa during the pumping process), and fill it with a 3MPa mixed gas containing carbon dioxide (V CO2 :V Ar =19:81), pumping and inflating again, after repeating 5 times, there is no hydrogen residue in the reactor, and the mixed gas containing carbon dioxide of 3MPa (V CO2 :V Ar =19:81), the reactor was placed at 180°C for reaction, after 40 hours of reaction, the reactor was cooled to room temperature, and the Ni@LaCO 3 OH composite material;
[0053] (3) Take out all the remaining gas in the kettle, ...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More