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Silver nanowire/nano gold composite electrode based on PDMS and preparation method thereof

A technology of silver nanowires and composite electrodes, applied in the direction of material electrochemical variables, etc., can solve the problems of high price, limited indium element reserves, non-bendability, etc., and achieve high mechanical properties, low resistance, and good application prospects.

Inactive Publication Date: 2019-02-01
DALIAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the currently widely used transparent conductive material indium tin oxide has limited reserves of indium element, is expensive, and cannot be bent by itself, while nano-silver wire has good bending resistance, electrical conductivity, and thermal conductivity, and is ideal for making flexible transparent conductive materials. good choice for

Method used

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  • Silver nanowire/nano gold composite electrode based on PDMS and preparation method thereof
  • Silver nanowire/nano gold composite electrode based on PDMS and preparation method thereof
  • Silver nanowire/nano gold composite electrode based on PDMS and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] (1) Fabrication of PDMS (polydimethylsiloxane) substrates. The substrate is fabricated by photolithography. Firstly, electronic drawing software is used to design the electrode drawing, and the drawing is printed as a mask plate by photolithography plate-making process, and then the photoresist is spin-coated on the surface of the clean silicon wafer to cover the mask plate containing the electrode pattern, and finally exposure and development are carried out , to obtain a silicon wafer template. Put it in a disposable petri dish; pour a PDMS mixed solution with a mass ratio of 10:1 on it; then put it in a vacuum desiccator to vacuum out the air bubbles in the PDMS mixed solution for 2 hours; take it out and put it in Heating and curing in a constant temperature oven at 80°C for 1 h; the finished substrate was treated with 3M adhesive tape (purchased from 3M Company in the United States) to remove the dust attached to the surface, and then put into an ultraviolet ozone...

Embodiment 2

[0036] (1) Fabrication of PDMS substrate. The substrate is fabricated by photolithography. First, electronic drawing software is used to design the electrode drawing, and the drawing is printed as a mask plate by photolithography plate-making process, and then the photoresist is spin-coated on the surface of the clean silicon wafer to cover the mask plate containing the electrode pattern, and finally exposure and development are carried out , to obtain a silicon wafer template. Put it in a disposable petri dish; pour a PDMS mixed solution with a mass ratio of 10:1 on it; then put it in a vacuum desiccator to vacuum out the air bubbles in the PDMS mixed solution for 2 hours; take it out and put it in Heating and curing in a constant temperature oven at 80°C for 1 h; the finished substrate was treated with 3M adhesive tape to remove the dust attached to the surface, and then placed in an ultraviolet ozone cleaner for 10 min to obtain a PDMS substrate with a fixed shape groove. ...

Embodiment 3

[0042] (1) Fabrication of PDMS (polydimethylsiloxane) substrates. Firstly, electronic drawing software is used to design the electrode drawing, and the drawing is printed as a mask plate by photolithography plate-making process, and then the photoresist is spin-coated on the surface of the clean silicon wafer to cover the mask plate containing the electrode pattern, and finally exposure and development are carried out , to obtain a silicon wafer template. Put it in a disposable petri dish; pour a PDMS mixed solution with a mass ratio of 10:1 on it; then put it in a vacuum desiccator to vacuum out the air bubbles in the PDMS mixed solution for 2 hours; take it out and put it in Heating and curing in a constant temperature oven at 80°C for 1 h; the finished substrate was treated with 3M adhesive tape to remove the dust attached to the surface, and then placed in an ultraviolet ozone cleaner for 10 min to obtain a PDMS substrate with a fixed shape groove.

[0043] (2) PDMS hydro...

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Abstract

The invention relates to a silver nanowire / nano gold composite electrode based on PDMS and a preparation method thereof. The silver nanowire / nano gold composite electrode based on PDMS comprises that:the PDMS is used for a substrate, silver nanowires are used for a conductive layer, and nano gold particles are used for an electrochemical deposition layer, the gold nanoparticles are deposited on the silver nanowires. The silver nanowire / nano gold composite electrode has the characteristics of low resistance and high mechanical property. The resistance range is 0.5 omega sq<-1> to 11 omega sq<-1>, the resistance range after bending 500 is 0.9 omega sq<-1> to 16 omega sq<-1>, and the resistance range after 100 times of stretching is 0.8 omega sq<-1> to 10 omega sq<-1>. The performance is ina prior level in the same industry, and has a good application prospect in the miniaturization and integration of electronic components.

Description

technical field [0001] The invention relates to the field of electrochemical sensors, in particular to a PDMS-based flexible silver nanowire / nano gold composite electrode and a preparation method thereof. Background technique [0002] Nowadays, flexible transparent electrodes play a pivotal role in the development of electronics and optoelectronics industries, and are indispensable optoelectronic functional materials for the preparation of many electronic and optoelectronic components. However, the currently widely used transparent conductive material indium tin oxide has limited reserves of indium element, is expensive, and cannot be bent by itself, while nano-silver wire has good bending resistance, electrical conductivity, and thermal conductivity, and is ideal for making flexible transparent conductive materials. good choice. [0003] Nanogold has unique physical and chemical properties, and its excellent optical, chemical, physical, electrical properties and biological...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N27/30G01N27/48
CPCG01N27/30G01N27/48
Inventor 孙晶甄雪郑则健郎明非
Owner DALIAN UNIV