Heavy metallic mineral thermosetting resin coated sand, preparation method and application thereof

A technology of resin coating and mineralization, which is applied in chemical instruments and methods, earthwork drilling, and drilling compositions, etc., can solve problems such as casing corrosion, affecting casing strength, and shortening the effective period of sand control. The effect of good temperature and wide source

Active Publication Date: 2019-02-22
PETROCHINA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in the investigation of the sand control effect of heavy oil steam huff and puff wells in Liaohe Oilfield, it was found that conventional fracturing sand control methods cannot maintain multiple rounds of steam huff and puff. worsening, the effective period of sand control is shortened, and the conventional coated sand is cured with hydrochloric acid, which will corrode the casing, affect the strength of the casing, and accelerate the damage of the casing

Method used

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  • Heavy metallic mineral thermosetting resin coated sand, preparation method and application thereof
  • Heavy metallic mineral thermosetting resin coated sand, preparation method and application thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0082] This embodiment provides a kind of heavy metal mineralization thermosetting resin coated sand, which is prepared by the following steps:

[0083] 1. Preparation of heavy metal mineralization particles

[0084] After crushing the raw material of heavy metal mineralization, sieve the raw material of 30 meshes; then dry it at 150°C for 5 hours; when drying, pass air into the oven to remove dust, control the content of fine powder below 0.3wt%, and obtain heavy metal mineralization particles. A slag rich in copper oxide and silicon carbide;

[0085] Wherein, the slag is slag resistant to steam corrosion, and the slag is black particles with a particle size range of 0.4-1.25mm and a bulk density of 1.50-1.75g / cm 3 , sphericity ≥ 0.5, roundness ≥ 0.5, alkali solubility ≤ 5%;

[0086] Based on the total weight of the slag as 100%, the content of the copper oxide is 50-60wt%, and the content of the silicon carbide is 20-30wt%;

[0087] 2. Preparation of thermosetting resin ...

Embodiment 2

[0100] This embodiment provides a kind of heavy metal mineralization thermosetting resin coated sand, which is prepared by the following steps:

[0101] 1. Preparation of heavy metal mineralization particles

[0102] After crushing the raw material of heavy metal mineralization, sieve the raw material of 30 meshes; then dry it at 150°C for 5 hours; when drying, pass air into the oven to remove dust, control the content of fine powder below 0.3wt%, and obtain heavy metal mineralization particles. A slag rich in copper oxide and silicon carbide;

[0103] Wherein, the slag is slag resistant to steam corrosion, and the slag is black particles with a particle size range of 0.4-1.25mm and a bulk density of 1.50-1.75g / cm 3 , sphericity ≥ 0.5, roundness ≥ 0.5, alkali solubility ≤ 5%;

[0104] Based on the total weight of the slag as 100%, the content of the copper oxide is 50-60wt%, and the content of the silicon carbide is 20-30wt%;

[0105] 2. Preparation of thermosetting resin ...

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Abstract

The invention provides a heavy metallic mineral thermosetting resin coated sand, a preparation method and an application thereof. The heavy metallic mineral thermosetting resin coated sand contains heavy metallic mineral grains serving as a skeleton support material and thermosetting resin coating layers coated on the surfaces of the heavy metallic mineral grains, wherein the heavy metallic mineral grains are slags rich in copper oxide and silicon carbide; the thermosetting resin coating layers comprise a curing layer and a protecting layer from inner to outer; the curing layer is prepared from a thermosetting organic silicon modified phenolic resin, a thermosetting furan resin, a coupling reagent, a heat-resisting modifier and a blender; the protecting layer is a lubricant protecting layer. The heavy metallic mineral thermosetting resin coated sand is a sand control agent used for sand control technologies in the field of oil production engineering, serves as a heavy metallic mineraltype novel sand control agent with resistance to alkali steam corrosion at 350 DEG C and steam curing at above 120 DEG C, is capable of prolonging the guarantee period of sand control and is suitablefor sand control of thickened oil thermal recovery oil-water wells.

Description

technical field [0001] The invention relates to a heavy metal mineralization thermosetting resin-coated sand and a preparation method and application thereof, belonging to the technical field of oil well sand control in oil production engineering. Background technique [0002] Sand production in oil and water wells is a common problem in the development of unconsolidated sandstone reservoirs. Due to various comprehensive factors such as oil well exploitation and operation, the rock formation structure near the bottom of the well is damaged, resulting in part of the detached formation sand flowing into the wellbore together with the reservoir fluid, resulting in sand formation. Buried oil layer, wellbore and pipeline sand plugging, surface pipeline and oil storage tank sand accumulation; oil pump, plunger and other equipment abrasion; well wall collapse, casing deformation and damage. A series of hazards caused by sand production in oil wells not only increase the cost of cru...

Claims

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Application Information

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IPC IPC(8): C09K8/80C09D183/04C09D161/06C09D161/00C09D7/63C09D7/65
CPCC08L2201/08C08L2205/035C09D183/04C09K8/80C09K8/805C09D7/63C09D7/65C08L61/06C08L61/00C08L95/00C08K5/544
Inventor 鄢德华胡祎阚新伟徐恩金张建军吕民汪小平张新委张学钦杜建马丽丽姜利曹朋青常琳清丁一铭毕文文张继潇邹运
Owner PETROCHINA CO LTD
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