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Polyhexamethylene biguanide hydrochloride compound microencapsulated antibacterial finishing agent and preparation method thereof

A technology of polyhexamidine hydrochloride and antibacterial finishing agent is applied in the field of microcapsule antibacterial finishing agent compounded with polyhexabiguanide hydrochloride and its preparation field, which can solve the problems of poor washing resistance, poor broad-spectrum and the like, To achieve good washing resistance, improve washing fastness, high safety effect

Inactive Publication Date: 2019-02-22
福州盛世凌云环保科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] Although the above-mentioned prior art can be antibacterial to a certain extent, the antibacterial finishing agents in the above-mentioned prior art all have the problems of poor broad spectrum and poor washing resistance to varying degrees.

Method used

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  • Polyhexamethylene biguanide hydrochloride compound microencapsulated antibacterial finishing agent and preparation method thereof
  • Polyhexamethylene biguanide hydrochloride compound microencapsulated antibacterial finishing agent and preparation method thereof
  • Polyhexamethylene biguanide hydrochloride compound microencapsulated antibacterial finishing agent and preparation method thereof

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Experimental program
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Effect test

Embodiment 1

[0043] (1) Preparation of the core material: under the stirring condition of a high-speed shear emulsifier, add 0.5 part of polyhexabiguanide hydrochloride, 1 part of nano-copper ion, 1 part of 3-methyl-4-isopropylphenol to the water 5 parts, 5 parts of vinylbisstearamide, 2 parts of polysorbate 80, 4 parts of polyvinyl alcohol, after stirring for 20-30 minutes, reduce the stirring speed to obtain the core material, and set aside;

[0044] (2) preparation of shell material: 30 parts of polycarbophil and 15 parts of chitosan are dissolved in citric acid solution, add PVP ethanol solution, obtain shell material after fully dissolving, for subsequent use;

[0045] (3) Preparation of microcapsules: at 50°C, add the core material obtained in step (1) dropwise to the shell material obtained in step (2), stir evenly while adding dropwise, fully mix, and then The temperature was naturally lowered to 20°C, and finally a microcapsule antibacterial finishing agent compounded with polyhex...

Embodiment 2

[0047] (1) Preparation of the core material: under the stirring condition of a high-speed shear emulsifier, 3 parts of polyhexabiguanide hydrochloride, 2 parts of nano-copper ions, 3 parts of 3-methyl-4-isopropylphenol were added to the water part, 8 parts of glyceryl tristearate, 5 parts of sorbitan laurel, 7 parts of hydroxymethylcellulose, after stirring for 20-30 minutes, reduce the stirring speed to obtain the core material, and set aside;

[0048] (2) preparation of shell material: 50 parts of polycarbophil and 20 parts of chitosan are dissolved in citric acid solution, add PVP ethanol solution, obtain shell material after fully dissolving, standby;

[0049] (3) Preparation of microcapsules: at 60°C, add the core material obtained in step (1) dropwise to the shell material obtained in step (2), stir evenly while adding dropwise, fully mix, and then The temperature was naturally lowered to 20°C, and finally a microcapsule antibacterial finishing agent compounded with poly...

Embodiment 3

[0051] (1) Preparation of the core material: under the stirring condition of a high-speed shear emulsifier, add 1 part of polyhexabiguanide hydrochloride, 5 parts of nano-copper ions, 2 parts of 3-methyl-4-isopropylphenol to water 5 parts, 5 parts of dioctyl sodium sulfosuccinate, 10 parts of sorbitan oleate, 5 parts of hydroxymethyl cellulose, after stirring for 20-30 minutes, reduce the stirring speed to obtain the core material, and set aside;

[0052] (2) Preparation of shell material: 40 parts of carbomer and 30 parts of chitosan are dissolved in citric acid solution, PVP ethanol solution is added, fully dissolved to obtain shell material, and set aside;

[0053] (3) Preparation of microcapsules: at 60°C, add the core material obtained in step (1) dropwise to the shell material obtained in step (2), stir evenly while adding dropwise, fully mix, and then The temperature was naturally lowered to 25°C, and finally a microcapsule antibacterial finishing agent compounded with ...

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Abstract

The invention relates to a polyhexamethylene biguanide hydrochloride compound microencapsulated antibacterial finishing agent and a preparation method thereof. The antibacterial finishing agent comprises a core material and a shell material; the core material comprises polyhexamethylene biguanide hydrochloride, nanometer copper ions, 3-methyl-4-isopropylphenol, a dispersant, an emulsifying agent and a stabilizer; and the shell material is a mixed biological adhesive material composed of a synthesized biological adhesive material and chitosan. The antibacterial finishing agent has high efficiency, wide spectrum and washing resistance to various fabrics and is high in safety, simple in preparation process and low in cost.

Description

technical field [0001] The invention relates to the field of antibacterial finishing agents, in particular to a microcapsule antibacterial finishing agent compounded with polyhexabiguanide hydrochloride and a preparation method thereof. Background technique [0002] Antibacterial finishing agents can be mainly divided into three types: inorganic, organic and natural. The early antibacterial agents basically belonged to the organic series, and most of them were various complex compounds containing nitrogen, sulfur, chlorine and other elements. The main varieties were: quaternary ammonium salts, biguanides, alcohols, phenols, aldehydes, organometallics , pyridines, thiophenes, etc. This type of antibacterial agent has good short-term antibacterial effect, but most of them have the disadvantages of poor heat resistance stability and short service life. [0003] In the past ten years, the requirements for green environmental protection have become more and more stringent, and ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M23/12D06M15/37D06M15/03D06M15/263D06M13/152D06M11/00B01J13/02
CPCB01J13/02D06M11/00D06M13/152D06M15/03D06M15/263D06M15/37D06M16/00D06M23/12
Inventor 郭思源
Owner 福州盛世凌云环保科技有限公司
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