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Metal substrate with spherical feature array microstructure and construction method thereof

A construction method and metal matrix technology, applied in metal processing equipment, manufacturing tools, welding equipment, etc., can solve the problems of unfavorable bone cell adhesion, proliferation, differentiation, and osseointegration on smooth surfaces, and achieve easy scale production and processing The process is simple and the effect of reducing stress concentration

Active Publication Date: 2020-04-21
NANJING UNIV OF AERONAUTICS & ASTRONAUTICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The purpose of the present invention is to propose a metal substrate and its construction method for preparing a spherical feature array microstructure on the surface of the metal substrate, so as to solve the problem that the smooth surface is not conducive to the adhesion, proliferation, differentiation and osseointegration of bone cells

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  • Metal substrate with spherical feature array microstructure and construction method thereof
  • Metal substrate with spherical feature array microstructure and construction method thereof
  • Metal substrate with spherical feature array microstructure and construction method thereof

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Experimental program
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Embodiment 1

[0028] The microstructure construction method with spherical feature array proposed by the present invention is as follows:

[0029] The first step is to use Ti6Al4V titanium alloy as the base material, and use wire cutting to process the base material into a size of 60mm×25mm×3mm, and use No. 1 to No. 6 metallographic sandpaper to polish the surface of the base material until there is no scratch under the naked eye. Then it was mechanically polished until there were no obvious scratches under the metallographic microscope, and then in the mixed solution (volume ratio: HF:HNO 3 :H 2 O=1:1:2) Wash for 15 seconds to remove surface scale, then quickly rinse with distilled water, and dry for later use.

[0030] In the second step, a square area of ​​25mm×25mm is drawn in the center of the titanium plate, and a layer of Ag72Cu solder with a thickness of 0.3mm is evenly coated in it. A metal template with an aperture diameter of 0.5 mm and a spacing between apertures of 0.15 mm (c...

Embodiment 2

[0034] The microstructure construction method with spherical feature array proposed by the present invention is as follows:

[0035] The first step is to use Ti6Al7Nb titanium alloy as the base material, and use wire cutting to process the base material into a size of 60mm×25mm×3mm, and use metallographic sandpaper No. 1 to 6 to polish the surface of the base material until there is no scratch under the naked eye. Then it was mechanically polished until there were no obvious scratches under the metallographic microscope, and then in the mixed solution (volume ratio: HF:HNO 3 :H 2 O=1:1:2) Wash for 15 seconds to remove surface scale, then quickly rinse with distilled water, and dry for later use. After the pretreatment, the samples were sandblasted to 60 mesh.

[0036] In the second step, a square area of ​​25 mm × 25 mm is drawn in the center of the titanium plate, and a layer of Ag72Cu solder with a thickness of 0.4 mm is evenly coated in it. A metal template with an apert...

Embodiment 3

[0040] The preparation method of the spherical feature array microstructure of the present invention is as follows:

[0041] The first step is to use Ti6Al4V titanium alloy as the base material, and use wire cutting to process the base material into a size of 60mm×25mm×3mm, and use No. 1 to No. 6 metallographic sandpaper to polish the surface of the base material until there is no scratch under the naked eye. Then it was mechanically polished until there were no obvious scratches under the metallographic microscope, and then in the mixed solution (volume ratio: HF:HNO 3 :H 2O=1:1:2) Wash for 15 seconds to remove surface scale, then quickly rinse with distilled water, and dry for later use. After the pretreatment, the sample was subjected to 60-mesh sandblasting, and then the surface of the micro-nano secondary composite structure was obtained by an acidic two-step etching method. The acidic two-step etching method is as follows: after sandblasting, the sample first obtains t...

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Abstract

The invention discloses a metal matrix of an array microstructure with spherical characteristics and a construction method of the metal matrix. The construction method comprises the steps that (1) byadopting a metal material as the matrix, a sample is subjected to heat treatment in advance firstly, specifically, the sample is cleaned in a mixed solution to remove oxide skin, then washed with distilled water and dried for standby application; (2) the surface of the metal matrix material is uniformly coated with a layer of brazing filler metal; (3) the metal material surface coated with the layer of brazing filler metal is covered with a metal template, a certain array of pores are arranged in the template, and then metal microbeads with materials corresponding to those of the matrix are sequentially put into gaps of the metal template; and (4) the metal template is taken out slowly, the metal microbeads are welded to the surface of the metal matrix material through a brazing technologyat the high vacuum degree and the suitable welding temperature, and thus the complete and uniform microstructure with the spherical characteristics is formed. The treatment process is simple, the manufacturing cost is low, scale production is easy, the obtained structure and the matrix have high adhesive force, and the metal matrix has important application value in the aspect of biomedical implants.

Description

technical field [0001] The invention belongs to the technical field of surface treatment of metal substrates, in particular to a metal substrate with a spherical feature array microstructure on the metal surface and a construction method thereof. The metal surface with spherical feature array microstructure constructed by the invention has important practical significance for promoting the application of the metal matrix in the fields of biomedicine, aerospace, ships and the like. Background technique [0002] Natural bone tissue is composed of subcompact compact bone and porous cancellous bone, and the surface contains multi-level structures such as micron, submicron and nanometer [1] . Based on the principle of bionics, the surface of the implant with micro-nano structure is closer to the surface structure of natural bone tissue than the smooth surface, and it is also more conducive to the differentiation of bone cells and osseointegration [2-3] . In addition, studies h...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B23K1/008B23K1/20
CPCB23K1/008B23K1/20
Inventor 沈一洲陶杰卢阳贾振峰吴正维江家威许杨江山
Owner NANJING UNIV OF AERONAUTICS & ASTRONAUTICS