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Soluble ink melanin dispersible tablet and preparation method thereof

A kind of ink melanin and soluble technology, which is applied in the field of soluble ink melanin dispersible tablets and its preparation, can solve the problems of low human absorption rate, waste of manpower and material resources, and low purity, and achieve the effects of shortening efficiency, facilitating absorption, and improving purity

Inactive Publication Date: 2019-03-26
ALPHA FUJIAN BIOTECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] However, the existing melanin preparation process not only takes a long time to prepare melanin, but also has low purity, which leads to waste of manpower and material resources and low absorption rate of human body.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A soluble ink melanin dispersible tablet, comprising the following steps in sequence: (1) the cuttlefish ink sac is thawed at room temperature, the epidermal membrane and the internal reticular membrane are removed to obtain cuttlefish ink powder, after adding 2 times the volume of ice water and stirring overnight, Then centrifuge to take the precipitate, wash it several times, and obtain the first product of melanin after the precipitate is vacuum freeze-dried; (in this embodiment, the centrifugation adopts 8000×g centrifugation for 10-20min, and the temperature of the ice water is 0-4°C.)

[0025] (2) Compound enzyme hydrolysis: get the melanin sample that step (1) obtains, add distilled water, the mass ratio of described melanin sample and described distilled water is 1:10, add 6mol / LNaOH aqueous solution to adjust pH value to 2.5, will The above material is heated and kept at a constant temperature of 55°C, then acidic protease and papain are added to the material, a...

Embodiment 2

[0033] A soluble ink melanin dispersible tablet, comprising the following steps in sequence: (1) the cuttlefish ink sac is thawed at room temperature, the epidermal membrane and the internal reticular membrane are removed to obtain cuttlefish ink powder, after adding 2 times the volume of ice water and stirring overnight, Then centrifuge to take the precipitate, wash it several times, obtain the precipitate and obtain the primary product of melanin after vacuum freeze-drying;

[0034] (2) Composite enzyme hydrolysis: take the melanin sample obtained in step (1), add distilled water, the mass ratio of the melanin sample to the distilled water is 1:30, add 6mol / L NaOH aqueous solution to adjust the pH value to 3.5, and The above material is heated and kept at a constant temperature of 75°C, then acidic protease and papain are added to the material, and enzymatically hydrolyzed at 75°C for 1 hour, the mass ratio of the acidic protease to the melanin sample is 2:100, and the papain...

Embodiment 3

[0042] A soluble ink melanin dispersible tablet, comprising the following steps in sequence: (1) the cuttlefish ink sac is thawed at room temperature, the epidermal membrane and the internal reticular membrane are removed to obtain cuttlefish ink powder, after adding 2 times the volume of ice water and stirring overnight, Then centrifuge to take the precipitate, wash it several times, obtain the precipitate and obtain the primary product of melanin after vacuum freeze-drying;

[0043] (2) Composite enzyme hydrolysis: take the melanin sample obtained in step (1), add distilled water, the mass ratio of the melanin sample to the distilled water is 1:20, add 6mol / L NaOH aqueous solution to adjust the pH value to 3.0, and The above material is heated and kept at a constant temperature of 65°C, then acidic protease and papain are added to the material, and the temperature is kept at 65°C for 1-2h, the mass ratio of the acidic protease to the melanin sample is 1:100, and the papain T...

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PUM

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Abstract

The invention relates to a soluble ink melanin dispersible tablet. A preparation method of the soluble ink melanin dispersible tablet comprises the following steps of (1) cleaning, (2) complex enzymehydrolysis, (3) ultrasonic preparation of soluble ink melanin and (4) tablet preparation, wherein the steps are carried out in sequence. Compared with the prior art, the soluble ink melanin dispersible tablet has the following beneficial effects that (1) the ink melanin extracted by an ultrasonication method under alkaline conditions is the soluble ink melanin which is more beneficial to human absorption, so that the dispersible tablet is enabled to exert greater health efficacy in a human body.

Description

technical field [0001] The invention relates to the technical field of food processing, in particular to a soluble ink melanin dispersible tablet and a preparation method thereof. Background technique [0002] Cephalopoda is a phylum of molluscs, a general term for species of cephalopods. The body is left and right symmetrical with a well-developed head and a pair of well-developed eyes on both sides. According to statistics, there are more than 700 species, all of which are marine products, such as octopus and squid, commonly known as cuttlefish, Calamari is commonly known as squid, nautilus, etc. Among them, the fishing volume of cuttlefish in my country is about 4 million tons a year, and its life cycle is short and its production speed is fast. It is known as one of the world's three underutilized and developed resources with great potential, so it develops rapidly . [0003] Melanin is a water-insoluble irregular biomacromolecule polymer, which widely exists in cuttlef...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L33/00A23P10/28
CPCA23V2002/00A23L33/00A23P10/28A23V2200/30
Inventor 高益槐唐文波戴金玉郑春源李小娟廖祖华
Owner ALPHA FUJIAN BIOTECH
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