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Yarn dyeing method for reduced dye

A technology for dyeing and dyeing yarn, applied in the direction of dyeing method, textile and papermaking, fiber processing, etc., can solve the problems of easy to produce color pattern, complicated operation, yarn color pattern, etc., and achieve bright color, complicated operation and uniform color. Effect

Inactive Publication Date: 2019-03-29
GUANGDONG ESQUEL TEXTILES CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method is cumbersome to operate, and it is easy to produce color flowers, so vat dyes are generally only used in dyeing cloth at present.
Many domestic textile enterprises have tried to apply vat dyes to dyeing yarns (such as bobbins and warp yarns of woven fabrics), but due to the serious problem of yarn coloring, there is no successful precedent.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] This embodiment is a method for dyeing yarn with vat dyes. In a dyeing vat with a diameter of 1800MM, a cylinder of 50S pure cotton cheese is cast and dyed. The cheese is a regular cylinder, and the density of the cheese in the same cylinder is basically the same. 0.37g / cm 3 , The bath ratio is 1:7.3, and the vat dye formula is: Shihlin Brilliant Green 0.0095% OWF, Shihlin Blue 0.326% OWF.

[0040] Proceed as follows:

[0041] 1. Pretreatment: After the bobbin is put into the vat, the main vat is filled with water, adding 0.9g / L scouring agent, 0.8g / L chelating dispersant, 0.8g / L hydrogen peroxide stabilizer, 3.0g / L 50% liquid caustic soda, 27.5 %H 2 o 24.5g / L, heat up to 110°C for 30 minutes; drain, then add water, add HAC 0.8g / L for pickling, and treat at room temperature for 5 minutes; drain, then add water, add 0.15g / L enzyme water to deoxygenate, and treat at room temperature for 5 minutes; drained, to be dyed;

[0042] 2. Dyeing—reduction: after the pretreatm...

Embodiment 2

[0047] This embodiment is a method for dyeing yarn with vat dyes. In a dyeing vat with a diameter of 1400MM, a vat of 40S pure cotton warp beam is cast and dyed, and the shaft surface is smooth, the yarn weight is 213.15KG, and the axial density is 0.47g / cm 3 , The bath ratio is 1:11.59, and the vat dye formula is: Shihlin Blue 0.0036% OWF, Shihlin Olive Green 0.205% OWF, Shihlin Purple 0.073% OWF.

[0048] Proceed as follows:

[0049] 1. Pre-treatment: After the warp yarn is put into the vat, the main vat is filled with water, adding 0.9g / L scouring agent, 0.8g / L chelating dispersant, 0.8g / L hydrogen peroxide stabilizer, 3.0g / L 50% liquid caustic soda, 27.5%H 2 o 2 4.5g / L, heat up to 110°C for 30 minutes; drain, then add water, add HAC 0.8g / L for pickling, and treat at room temperature for 5 minutes; drain, then add water, add 0.15g / L enzyme water to deoxygenate, and treat at room temperature for 5 minutes; drained, to be dyed;

[0050] 2. Dyeing—reduction: after the pret...

Embodiment 3

[0055] A method for dyeing yarn with vat dyes in this embodiment, its raw materials and steps are the same as in Example 1, the difference is that step 3 dyeing—the oxidation process is as follows:

[0056] Cool down the main vat to 50°C, run for 15 minutes, reduce the pump speed to the requirement, return the dye solution to the material vat in the main vat, test the foot water with yellow test paper, make sure the yellow test paper turns blue, then add dispersant 1.0g / L and weak oxidant 2.0g / L, after a little stirring, pump it into the main vat, run at 50°C for 15 minutes, then reflux, add hydrogen peroxide 2.0g / L, then pump it into the main vat, continue to run at 50°C for 15 minutes, and drain.

[0057] The inside and outside color difference of the package yarn dyed by the above method: Delta E 0.57, colorless, no tube picking. There is no feedback on the quality of internal and external differences in subsequent processing and use procedures; in terms of color fastness: ...

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Abstract

The invention relates to a yarn dyeing method for a reduced dye. The yarn dyeing method comprises the following steps: carrying out pretreatment on yarns; adding water and the reduced dye into the yarns after pretreatment, and then adding alkaline and a reducing agent for a reduction reaction; after the reduction reaction is finished, adding a weak oxidant for treatment for 5 to 15 min at the temperature of 50 to 70 DEG C, and then adding a strong oxidant for treatment for 5 to 15 min for an oxidation reaction; and carrying out aftertreatment on the yarn after the oxidation reaction. The yarndyeing method can effectively solve the problems, such as dyeing defect and color difference between inner and outer layers, of the reduced dye used for yarn dyeing, so that the obtained yarn is uniform in color, bright in color and high in soaping and light fastness.

Description

technical field [0001] The invention relates to the technical field of textiles, in particular to a method for dyeing yarn with vat dyes. Background technique [0002] Vat dyes are dyes with excellent properties in dyes. According to its main chemical structure, it can be divided into two categories: indigo and anthraquinone. It has a relatively complete chromatogram, bright color, and high fastness to soaping and sunlight. The dyeing process is as follows: first, it becomes a soluble leuco-salt through reduction in lye, which is adsorbed by the cellulose fiber, and then oxidized to return to the original insoluble dye. [0003] Traditional vat dyeing generally adopts the "dry vat method (pre-reduction method)", that is, vat dyes are first reduced, and then added to the dye vat for dyeing. This method is cumbersome to operate and is prone to color flowers, so vat dyes are generally only applied to dyed cloth at present. Many domestic textile enterprises try to apply vat ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/22D06P5/10D06P5/04D06L4/13D06L4/12D06M13/188D06M16/00
CPCD06M13/188D06M16/003D06P1/22D06P5/04D06P5/10D06L4/12D06L4/13
Inventor 黎娟何韵湘安志轩陈晓霓吴海彬
Owner GUANGDONG ESQUEL TEXTILES CO LTD