Porous amorphous soft magnetic composite wave-absorbing material and preparation method thereof
A soft magnetic composite material and a composite material technology are applied to a porous iron-based amorphous soft magnetic alloy composite wave absorbing material. The field of preparation of the wave absorbing material can solve the problems of limited in-depth application, high dielectric constant of magnetic metal micropowder, and difficulty in Impedance matching and other issues, to achieve the effects of excellent soft magnetic performance, good thermal stability and low cost
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Embodiment 1
[0040] A preparation method of FeSiBPC / graphite composite wave-absorbing material, comprising the steps of:
[0041] Step 1: Fe 76 Si 7.6 B 9.5 P5C 1.9 Alloy atomic percent is converted into weight percent, Fe, Si and FeB, FeP and FeC alloy raw materials are weighed in proportion, and set aside.
[0042] Step 2: Put the mixture according to the above-mentioned composition ratio in the graphite crucible of the induction melting furnace, and first evacuate to 10 -3 Pa, then fill it with argon to a pressure of 500mbar, continue melting for 30 seconds after melting, then let the alloy cool down to room temperature with the crucible, repeat melting 3 times, and then cast it into a copper mold to obtain a uniform alloy ingot.
[0043] Step 3: Break the spindle obtained in Step 2 into small pieces, and place them in alcohol for ultrasonic cleaning.
[0044] Step 4: Put the small piece of alloy obtained in step 3 into a quartz glass tube with an open lower end, and then put it in...
Embodiment 2
[0050] A preparation method of FeSiBPC / graphite composite wave-absorbing material, comprising the steps of:
[0051] Step 1: Fe 76 Si 7.6 B 9.5 P 5 C 1.9 Alloy atomic percent is converted into weight percent, Fe, Si and FeB, FeP and FeC alloy raw materials are weighed in proportion, and set aside.
[0052] Step 2: Put the mixture according to the above-mentioned composition ratio in the graphite crucible of the induction melting furnace, and first evacuate to 10 -3 Pa, then fill it with argon to a pressure of 500mbar, continue melting for 30 seconds after melting, then let the alloy cool down to room temperature with the crucible, repeat melting 3 times, and then cast it into a copper mold to obtain a uniform alloy ingot.
[0053] Step 3: Break the spindle obtained in Step 2 into small pieces, and place them in alcohol for ultrasonic cleaning.
[0054] Step 4: Put the small piece of alloy obtained in step 3 into a quartz glass tube with an open lower end, and then put it...
Embodiment 3
[0061] A preparation method of FeSiBPC / graphite composite wave-absorbing material, comprising the steps of:
[0062] Step 1: Fe 76 Si 7.6 B 9.5 P 5 C 1.9 Alloy atomic percent is converted into weight percent, Fe, Si and FeB, FeP and FeC alloy raw materials are weighed in proportion, and set aside.
[0063] Step 2: Put the mixture according to the above-mentioned composition ratio in the graphite crucible of the induction melting furnace, and first evacuate to 10 -3 Pa, then fill it with argon to a pressure of 500mbar, continue melting for 30 seconds after melting, then let the alloy cool down to room temperature with the crucible, repeat melting 3 times, and then cast it into a copper mold to obtain a uniform alloy ingot.
[0064] Step 3: Break the spindle obtained in Step 2 into small pieces, and place them in alcohol for ultrasonic cleaning.
[0065] Step 4: Put the small piece of alloy obtained in step 3 into a quartz glass tube with an open lower end, and then put it...
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