Resin composition for power storage device electrode
A technology of resin composition and power storage equipment, which is applied to battery electrodes, non-aqueous electrolyte storage battery electrodes, hybrid capacitor electrodes, etc., which can solve the problems of poor durability, reduced capacity, and damaged ion conductivity, etc., and achieve improved battery performance. properties, good adhesion, and excellent ion permeability
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example 1
[0267] The polymer particle dispersions of Examples 1 to 4 and Comparative Example 1 shown in Table 1 were prepared using the following raw materials. The abbreviations of the raw materials used in Table 1 and the following examples are as follows.
[0268]
[0269] MMA: methyl methacrylate (manufactured by Wako Pure Chemical Industries, Ltd.)
[0270] EA: Ethyl acrylate (manufactured by Wako Pure Chemical Industries, Ltd.)
[0271] BA: butyl acrylate (manufactured by Wako Pure Chemical Industries, Ltd.)
[0272] 2-EHA: 2-ethylhexyl acrylate
[0273]
[0274] AA: Acrylic acid (manufactured by Wako Pure Chemical Industries, Ltd.)
[0275]
[0276] EGDMA: Ethylene glycol dimethacrylate (manufactured by Wako Pure Chemical Industries, Ltd.)
[0277]
[0278] APS: ammonium persulfate
[0279] KPS: potassium persulfate
[0280]
[0281] Na: sodium
[0282] Li: Lithium
[0283] NH 4 : Ammonium
[0284]
[0285] Sodium dodec...
Embodiment 1
[0286] [Polymer particle dispersion of Example 1]
[0287] 194 g of EA as the monomer (A-1), 6 g of AA as the monomer (B-1), 0.20 g of EGDMA as the monomer (C) [relative to the monomers (A-1) and (B-1) The total number of moles is 0.1 mol%] and 340 g of ion-exchanged water were added to a glass four-necked separable flask with an inner capacity of 1 L, and stirred for a predetermined time (0.5 hours) under a nitrogen atmosphere. Next, after raising the temperature of the reaction solution in the flask to around 70°C, a polymerization initiator solution in which 1 g of APS was dissolved in 10 g of ion-exchanged water was added to the flask, and the reaction solution in the flask was kept at around 70 to 75°C. For 6 hours, the polymerization and aging proceeded to obtain a polymer particle dispersion. Thereafter, the polymer particle dispersion in the flask was cooled to room temperature, and after adding 29.14 g of 1N LiOH aqueous solution to neutralize, the aggregate was ...
Embodiment 2
[0288] [Polymer particle dispersion of Example 2]
[0289] Obtained in the same manner as in Example 1 except that the amount of the monomer (C) used was changed to 1.0 g [0.5 mol% relative to the total number of moles of the monomers (A-1) and (B-1)] Polymer Particle Dispersion of Example 2. Table 1 shows the amount and type of each component used in the preparation of the polymer particle dispersion of Example 2.
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