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Water-soluble compound fertilizer anti-caking agent and method for preparing same

A water-soluble compound and anti-caking agent technology, applied in fertilizer mixtures, fertilization devices, applications, etc., can solve problems such as blocking nozzles, affecting users' use, and easy caking of products, and achieves the effect of fast water solubility.

Inactive Publication Date: 2019-04-05
无锡市天膜新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in order to achieve high nitrogen, high potassium and full water solubility of fully water-soluble compound fertilizers, the raw materials generally include urea, ammonium phosphate, ammonium nitrate, ammonium nitrate phosphorus, potassium chloride, potassium sulfate, etc. These raw materials have different degrees of hygroscopicity. The hygroscopicity will change after the raw materials are mixed. Improper selection of raw materials will reduce the hygroscopic point and enhance the hygroscopicity, which will cause the product to agglomerate easily during storage.
[0003] Although the traditional anti-coagulation agent can play an anti-coagulation effect, it will produce insoluble matter after the water-soluble compound fertilizer is dissolved, especially when the nozzle is blocked during drip irrigation, which affects the use of users.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] A water-soluble compound fertilizer anticaking agent comprises the following components in weight percentage: 85 parts of polymer surfactant, 15 parts of fatty acid derivative and 5 parts of polycarbonate alcohol.

[0016] The polymer surfactant is PEG-50 sorbitol, and the fatty acid derivative is fatty ester.

[0017] The fatty ester is a mixture of methyl dodecanoate, methyl 5-dodecenoate and methyl myristate.

[0018] A preparation method of a water-soluble composite fertilizer anti-caking agent, comprising the following steps: first adding a polymer surfactant to a reactor and heating it to 110°C, adding polycarbonate alcohol in proportion and keeping it warm for 20 minutes, and then adding fatty acid derivatives Add the reaction kettle to control the temperature at 70°C, and then enter the high-speed stirring and emulsifying equipment for high-speed stirring for 30 minutes, so that the product is fully emulsified and the finished product is produced.

Embodiment 2

[0020] A water-soluble compound fertilizer anticaking agent comprises the following components in parts by weight: 95 parts of a polymer surfactant, 10 parts of a fatty acid derivative, and 0.5 part of a polycarbonate alcohol.

[0021] The polymer surfactant is a mixture of polyethylene glycol 600-vinylidene chloride graft copolymer and polydimethylacrylamide-n-butyl acrylate graft polymer in a volume ratio of 2:1.

[0022] The fatty acid derivative is a mixture of methyl 7-tetradecenoate, methyl 9-hexadecenoate and methyl 11-octadecenoate.

[0023] A preparation method of a water-soluble composite fertilizer anti-caking agent, comprising the following steps: first adding a polymer surfactant to a reactor and heating it to 120° C., adding polycarbonate alcohol in proportion and keeping it warm for 20 minutes, and then adding fatty acid derivatives Add the reaction kettle to control the temperature at 65°C, and then enter the high-speed stirring and emulsifying equipment for hi...

Embodiment 3

[0025] A water-soluble compound fertilizer anticaking agent comprises the following components in parts by weight: 90 parts of a polymer surfactant, 12 parts of fatty acid derivatives, and 3 parts of polycarbonate alcohols.

[0026] The polymer surfactant is polyalkylene oxide; the fatty ester is a mixture of methyl dodecanoate, methyl myristate, methyl hexadecanoate and methyl octadecanoate.

[0027] A preparation method of a water-soluble composite fertilizer anti-caking agent, comprising the following steps: firstly adding a polymer surfactant to a reactor and heating it to 105°C, adding polycarbonate alcohol in proportion and keeping it warm for 20 minutes, and then adding fatty acid derivatives Add the reaction kettle to control the temperature at 68°C, and then enter the high-speed stirring and emulsifying equipment for high-speed stirring for 30 minutes, so that the product is fully emulsified and the finished product is produced.

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PUM

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Abstract

The invention discloses a water-soluble compound fertilizer anti-caking agent and a method for preparing the same. The water-soluble compound fertilizer anti-caking agent comprises, by weight, 85-95 parts of polymeric surfactants, 10-15 parts of fatty acid derivatives and 0.5-5 parts of poly-carbon alcohol. The method includes adding the polymeric surfactants into reaction kettles and heating thepolymeric surfactants until the temperatures of the polymeric surfactants reach 110-120 DEG C; proportionally adding the poly-carbon alcohol into the reaction kettles and preserving heat for 20 minutes; adding the fatty acid derivatives into the reaction kettles and keeping the temperatures of 65-70 DEG C unchanged under the control; feeding products into high-speed stirring and emulsifying equipment, and stirring the products at the high speeds for 30 minutes; sufficiently emulsifying the products and then discharging the water-soluble compound fertilizer anti-caking agent which is a finishedproduct. The water-soluble compound fertilizer anti-caking agent and the method have the advantages that the water-soluble compound fertilizer anti-caking agent is high in water dissolution speed, isfree of residues after being dissolved, is convenient without being heated when used, is environmentally friendly and is free of pollution, and good anti-caking effects can be realized by the water-soluble compound fertilizer anti-caking agent.

Description

technical field [0001] The invention relates to a water-soluble composite fertilizer anticaking agent and a preparation method thereof. Background technique [0002] Fully water-soluble compound fertilizer is a multi-component compound fertilizer that can be completely dissolved in water. It can be quickly dissolved in water and is more easily absorbed by crops, and its absorption and utilization rate is relatively high. More importantly, it can be applied to Facility agriculture such as drip irrigation realizes the integration of water and fertilizer, and achieves the efficiency of saving water, fertilizer and labor. Because the fully water-soluble compound fertilizer has the characteristics of simple use method and convenient use, it has developed rapidly in our country in recent years. However, in order to achieve high nitrogen, high potassium and full water solubility of fully water-soluble compound fertilizers, the raw materials generally include urea, ammonium phospha...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C05G3/00
CPCC05G3/20
Inventor 高明福殷丽静杨招弟沈维兴高其芬
Owner 无锡市天膜新材料有限公司
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