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191 results about "Phosphorus acid" patented technology

Preparation method for wear resistant fire-retardant coating

The invention provides a preparation method for wear resistant fire-retardant coating with simple construction process, good wear resistance and relatively low cost. The raw material of the wear resistant fire-retardant coating selects plate-shaped tabular alumina, brown alumina and high-quality bauxite chamotte as aggregate, selects plate-shaped tabular alumina powder, flint clay powder, alpha-Al2O3 micropowder and ceramic powder as fine powder, selects 42.5 mass percent industrial phosphoric acid solution, solid aluminium dihydrogen phosphate and clay powder as bonding agents, selects fused magnesite as a curing agent and selects sodium borate and sodium hexametahposphate as sintering aids. The wear resistant fire-retardant coating can be directly smeared on the surfaces of a wear resistant fire-retardant material liner and a water cooling wall pipe, fills up technical blank of resisting the wear on metal by using a non metal coating at a high temperature of 900 DEG C, provides a new repairing method for a non metal wear resistant fire-retardant material liner, has simple construction process, can obviously improve working environment of workers, reduce the labor intensity and improve the working efficiency of maintaining a circulating fluid bed boiler heated surface metal pipe wall and the wear resistant fire-retardant material liner.
Owner:TONGDA REFRACTORY TECH CO LTD

Silver nanometer column array erected on orifice of porous alumina template and preparation method and application thereof

The invention discloses a silver nanometer column array erected on the orifice of a porous alumina template and a preparation method and application thereof. The silver nanometer column array is characterized in that silver nanometer columns with the heights of 30-200 nanometers and the diameters of 30-60 nanometers are sequentially hexagonally arrayed on the periphery of the orifice of the porous anodic alumina template with taper holes; and silver nanometer particles with the particle size of 5-40 nanometers are attached to the walls of the taper holes. The preparation method comprises the following steps of: firstly placing an aluminum sheet into an oxalic acid solution, and carrying out anodization at direct-current voltage for at least 2 hours; then placing into a phosphorus-chromium acid mixed solution, and soaking for at least 3 hours to obtain an intermediate product; then firstly placing the intermediate product into the oxalic acid solution, carrying out the anodization at the direct-current voltage for at least 20 seconds, then placing the intermediate product into a phosphorus acid solution, and soaking for at least 1 minute; repeating the process for at least 10 times to obtain the alumina template with the holes in the shape of the taper holes; and then placing the alumina template into an ion sputter for silver sputtering so as to prepare a target product. The silver nanometer column array disclosed by the invention can be used as an active base of surface-enhanced Raman scattering; and the content of rhodamine or tetrachlorobiphenyl which is attached to the silver nanometer column array is measured by using a laser Raman spectrometer.
Owner:HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI

Method for manufacturing low-pressure chemical synthesis foil for aluminum electrolysis capacitor and middle treatment groove

InactiveCN101235529ANo loss of capacitanceHigh passivation treatment efficiencyElectrolytic capacitorsPhosphatisationChemical synthesisElectricity
The invention relates to a method for forming foil by low voltage of an aluminum electrolytic capacitor and a treatment groove for forming foil, wherein the method comprises the following steps: placing the formed foil which is treated by forming treatment under the highest forming voltage into a medium treatment groove and a groove solution, and proceeding the medium treatment, then proceeding subsequent forming treatment, an electrode plate which is corresponded with the formed foil is arranged in the treatment groove, the groove solution comprises phosphorus acid and / or ammonium phosphate component, the medium treatment comprises the following steps: placing the anode of direct current power supply on the formed foil, placing the cathode of the direct current power supply on an electrode plate, imposing electricity to the forming foil, the voltage value of the imposing electrical treatment is lower than that of the highest formed. The forming method of the invention and the treatment groove has the advantages that the efficiency of deactivation treatment is high, the coverage of the deactivation treatment is more comprehensive and thoroughly, which can simultaneously obtain higher electrostatic capacity, good water resistance and hydratability.
Owner:乳源县立东电子科技有限公司
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