High temperature resistant boron nitride-cerium feldspar ceramic matrix composite material and preparation method thereof

A composite material, strontium feldspar technology, applied in the field of high temperature resistant boron nitride-strontium feldspar ceramic matrix composite material and its preparation, can solve the problems of low density, low thermal expansion coefficient, limited application of strontium feldspar, poor processability, etc. Achieve high density, inhibit abnormal grain growth, good dielectric and high temperature resistance

Active Publication Date: 2019-04-19
HARBIN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0002] Strontium feldspar has the advantages of low density, small thermal expansion coefficient, good high temperature stability, excellent dielectric properties and excellent chemical stability. It has a wide range of application pr

Method used

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  • High temperature resistant boron nitride-cerium feldspar ceramic matrix composite material and preparation method thereof
  • High temperature resistant boron nitride-cerium feldspar ceramic matrix composite material and preparation method thereof
  • High temperature resistant boron nitride-cerium feldspar ceramic matrix composite material and preparation method thereof

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Example Embodiment

[0032] In order to solve the problem of poor workability of strontium feldspar, the present invention provides a high-temperature resistant boron nitride-strontium feldspar ceramic matrix composite material and a preparation method of the composite material, see figure 1 As shown, the preparation method of the high temperature resistant boron nitride-strontium feldspar ceramic matrix composite material includes the following steps:

[0033] S1: Weigh and mix strontium feldspar powder and hexagonal boron nitride powder to obtain raw materials;

[0034] S2: Ball mill the raw materials to obtain ball mill powder;

[0035] S3: Stir and dry the ball mill powder to obtain raw material powder;

[0036] S4: After sieving the raw material powder, put it into a graphite mold and perform cold pressing to obtain a bulk raw material;

[0037] S5: Perform spark plasma sintering on the obtained bulk raw material to obtain a high temperature resistant boron nitride-strontium feldspar ceramic matrix com...

Example Embodiment

[0059] Example one

[0060] This embodiment provides a method for preparing a high-temperature resistant boron nitride-strontium feldspar ceramic matrix composite material, the method including:

[0061] S1: Weigh 77.35 g of strontium feldspar powder with a particle size of 200 mesh and 13.68 g of hexagonal boron nitride powder with a particle size of 100 mesh and a purity of 99% by weight and mix to obtain a raw material;

[0062] S2: Place the obtained raw materials in a polytetrafluoroethylene ball milling tank, use alumina balls as the ball milling medium, and add absolute ethanol for wet ball milling for 24 hours to obtain ball mill powder;

[0063] S3: Stir and dry the ball mill powder at 60°C for 4 hours to obtain raw material powder;

[0064] S4: Pass the raw material powder through a 100-mesh sieve and put it into a graphite mold, and cold press it at a pressure of 30 MPa for 3 minutes to obtain a bulk raw material;

[0065] S5: Perform spark plasma sintering on the bulk raw mat...

Example Embodiment

[0076] Example two

[0077] This embodiment provides a method for preparing a high-temperature resistant boron nitride-strontium feldspar ceramic matrix composite material, the method including:

[0078] S1: Weigh and mix 56.4 g of strontium feldspar powder with a particle size of 200 mesh and 37.6 g of hexagonal boron nitride powder with a particle size of 100 mesh and a purity of 99% by weight to obtain a raw material;

[0079] S2: Place the obtained raw materials in a polytetrafluoroethylene ball milling tank, use alumina balls as the ball milling medium, and add absolute ethanol for wet ball milling for 12 hours to obtain ball mill powder;

[0080] S3: Stir and dry the ball mill powder at 60°C for 6 hours to obtain raw material powder;

[0081] S4: Pass the raw material powder through a 100-mesh sieve and put it into a graphite mold with an inner diameter of 20 mm and coated with boron nitride on the inner wall, and cold press at a pressure of 15 MPa for 5 minutes to obtain a bulk r...

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Abstract

The invention discloses a high temperature resistant boron nitride-cerium feldspar ceramic matrix composite material and a preparation method thereof, and relates to the technical field of preparationof ceramic matrix composite materials. The preparation method comprises the steps of S1, weighing cerium feldspar powder to be mixed with hexagonal boron nitride powder to obtain a raw material; S2,ball-milling the raw material to obtain ball-milled powder; S3, stirring and drying the ball-milled powder to obtain raw material powder; S4, placing the raw material powder into a graphite mold, andcold-pressing is performed to obtain a bulk material; S5, performing discharge plasma sintering on the bulk material to obtain the high temperature resistant boron nitride-cerium feldspar ceramic matrix composite material. The preparation method of the high temperature resistant boron nitride-cerium feldspar ceramic matrix composite material has the advantages that the prepared boron nitride-cerium feldspar ceramic matrix composite material not only has good mechanical and processability performance by introducing boron nitride into cerium feldspar, but also has good dielectric and high temperature resistance performance.

Description

technical field [0001] The invention relates to the technical field of preparation of ceramic-based composite materials, in particular to a high-temperature-resistant boron nitride-strontium feldspar ceramic-based composite material and a preparation method thereof. Background technique [0002] Strontium feldspar has the advantages of low density, small thermal expansion coefficient, good high temperature stability, excellent dielectric properties and excellent chemical stability. It has wide application prospects; however, due to its excellent thermal and dielectric properties, strontium feldspar also has the characteristics of poor processability, which greatly limits the application of strontium feldspar in practical engineering. [0003] In view of the above-mentioned defects, the creator of the present invention has finally obtained the present invention through long-term research and practice. Contents of the invention [0004] In order to solve the above-mentioned...

Claims

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Application Information

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IPC IPC(8): C04B35/195C04B35/622C04B35/64
CPCC04B35/195C04B35/622C04B35/64C04B2235/386C04B2235/666
Inventor 蔡德龙贾德昌杨治华段小明何培刚王胜金周玉
Owner HARBIN INST OF TECH
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