UV (ultraviolet) curing glue with high glass-transition temperature
A technology with transition temperature and high vitrification, applied in the field of curing glue, can solve the problems of low production efficiency, high cost, consumption, etc., and achieve the effect of physical protection and high hardness
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Embodiment 1
[0019] Embodiment 1: According to 3,4-epoxycyclohexylmethyl-3, the mass percent of 4-epoxycyclohexane carbonate is 65%, the mass percent of polycaprolactone is 32%, hexafluoroantimonate The mass percentage is 0.9%, and each raw material is added in turn, after adding the fumed silicon micropowder of 2% by mass, after defoaming and stirring, then adding 0.1% of the pigment whose absorption spectrum peak is 450~495nm visible light ( The pigment is shown as blue), after defoaming and stirring, it is filtered through a 200-mesh metal sieve and packed into a can. Use Philips 18-watt ultraviolet light for photocuring. The distance between the lamp and the sample is about 5 cm. When the sample with a thickness of about 0.5-0.6 mm completely changes from liquid to solid, it is called the time required for curing. It needs to be placed at room temperature for 24 hours, and the post-curing is completed, and the hardness will be slightly higher than when the light is completed. The hard...
Embodiment 2
[0020] Embodiment 2: According to 3, the mass percent of 4-epoxycyclohexylmethyl-3,4-epoxycyclohexane carbonate is 65%, the mass percent of polycaprolactone is 32%, hexafluoroantimonate The mass percentage is 0.9%, and each raw material is added in turn, after adding the fumed silicon micropowder of 2% by mass, after defoaming and stirring, then adding 0.1% of the pigment whose absorption spectrum peak is 495~570nm visible light ( The pigment is shown as green), after defoaming and stirring, it is filtered through a 200-mesh metal sieve, and canned. Use Philips 18-watt ultraviolet light for photocuring. The distance between the lamp and the sample is about 5 cm. When the sample with a thickness of about 0.5-0.6 mm completely changes from liquid to solid, it is called the time required for curing. It needs to be placed at room temperature for 24 hours, and the post-curing is completed, and the hardness will be slightly higher than when the light is completed. The hardness was ...
Embodiment 3
[0021] Embodiment 3: According to 3,4-epoxycyclohexylmethyl-3, the mass percent of 4-epoxycyclohexane carbonate is 65%, the mass percent of polycaprolactone is 32%, hexafluoroantimonate The mass percentage is 0.9%, each raw material is added in turn, after adding the fumed silicon micropowder which is 2% by mass, after defoaming and stirring, then add 0.1% by mass of the pigment of 570-590nm visible light (the pigment is shown as Yellow), defoamed and stirred evenly, filtered through a 200-mesh metal sieve, and packed into cans. Use Philips 18-watt ultraviolet light for photocuring. The distance between the lamp and the sample is about 5 cm. When the sample with a thickness of about 0.5-0.6 mm completely changes from liquid to solid, it is called the time required for curing. It needs to be placed at room temperature for 24 hours, and the post-curing is completed, and the hardness will be slightly higher than when the light is completed. The hardness was tested with a Shore D...
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