Method for preparing high-thermal-conductivity silicon nitride ceramic

A technology of silicon nitride ceramics and silicides, which is applied in the field of preparation of silicon nitride ceramic materials with high thermal conductivity, and can solve the problems of difficult preparation, high cost, harmful fluoride gas, etc.
CN109851369AActive Publication Date: 2019-06-07江西中科上宇科技有限公司

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
江西中科上宇科技有限公司
Publication Date
2019-06-07

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Abstract

The invention relates to a method for preparing silicon nitride ceramic with high thermal conductivity, which comprises the following steps: uniformly mixing alpha-Si3N4 powder with a sintering aid, and carrying out compression molding to obtain a green body; and carrying out gas pressure sintering on the green body at the temperature of 1780-1950 DEG C in an inert atmosphere, and then cooling thesintered product to room temperature to obtain the silicon nitride ceramic; wherein the sintering aid is composed of silicide and alkaline earth metal oxide, the ratio of the alpha-Si3N4 powder to the sintering aid being (90mol%) : (10mol%) - (99mol%) : (1mol%).
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Description

technical field

[0001] The invention relates to a preparation method of a silicon nitride ceramic material with high thermal conductivity, belonging to the field of inorganic non-metallic materials. Background technique

[0002] With the development of semiconductor devices in the direction of integration, miniaturization, and high power, device heat dissipation has become one of its important technical bottlenecks. Solving the heat dissipation problem largely depends on the performance of the ceramic substrate in the device. Currently commonly used ceramic heat dissipation substrates are alumina (Al 2 o 3 ), aluminum nitride (AlN), silicon carbide (SiC), beryllium oxide (BeO), etc. where Al 2 o 3 The thermal conductivity of ceramics is the lowest, and its expansion coefficient is greatly different from that of silicon components; AlN and BeO have the best thermal conductivity, but BeO powder is highly toxic; AlN has poor mechanical properties; SiC ceramics have low ins...

Claims

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