Graphene modified oxidized polyethlene wax emulsion and preparing method thereof
An oxidized polyethylene wax and graphene modification technology, applied in textiles, papermaking, fiber processing, etc., can solve the problems of unstable performance and poor dispersion, and achieve the effect of improving cutting resistance, avoiding pollution and simple process.
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Embodiment 1
[0033] The graphene-modified oxidized polyethylene wax emulsion provided in this embodiment includes: graphene 5g, isomeric tridecyl alcohol polyoxyethylene ether (EO number is 6) 15g, low-density oxidized polyethylene wax 20g, 5g stearyl alcohol , 54.8g of water and 0.2g of triethanolamine.
[0034] The preparation method of the graphene-modified oxidized polyethylene wax emulsion provided by the present embodiment comprises the following steps:
[0035] Step (1), preparing an emulsification kettle with a fractionation device, is provided with a thermometer, a stirrer and a nitrogen inlet pipe in the emulsification kettle;
[0036] Step (2), successively drop into graphene 5g, isomerized tridecyl alcohol polyoxyethylene ether (EO number is 6) 15g, low-density oxidized polyethylene wax 20g, 5g stearyl alcohol, 54.8g water and triethanolamine 0.2g;
[0037] Step (3), input nitrogen gas from the nitrogen gas inlet pipe, under the protection of nitrogen gas, start the stirrer, s...
Embodiment 2
[0043] The difference between this embodiment and embodiment 1 is:
[0044] The graphene-modified oxidized polyethylene wax emulsion provided in this embodiment includes: 2 g of single-layer graphene, 15 g of isomeric tridecyl alcohol polyoxyethylene ether (EO number is 6), 25 g of high-density oxidized polyethylene wax, 3 g of ten Octanol, 54.8 g of water and 0.2 g of potassium hydroxide.
[0045] The preparation method of the graphene-modified oxidized polyethylene wax emulsion provided by the present embodiment comprises the following steps:
[0046] Step (1), preparing an emulsification kettle with a fractionation device, is provided with a thermometer, a stirrer and a nitrogen inlet pipe in the emulsification kettle;
[0047] Step (2), drop in successively 2g of single-layer graphene, isomeric tridecyl alcohol polyoxyethylene ether (EO number is 6) 15g, high-density oxidized polyethylene wax 25g, 3g stearyl alcohol, 54.8g water and potassium hydroxide 0.2g;
[0048] St...
Embodiment 3
[0054] The differences between this embodiment and embodiment 1 and embodiment 2 are:
[0055] The graphene-modified oxidized polyethylene wax emulsion provided in this embodiment includes: graphene oxide 5g, isomeric tridecyl alcohol polyoxyethylene ether (EO number is 8) 15g, high-density oxidized polyethylene wax 25g, 5g octadecanol Alcohol, 49.8g of water and 0.2g of potassium hydroxide.
[0056] The preparation method of the graphene-modified oxidized polyethylene wax emulsion provided by the present embodiment comprises the following steps:
[0057] Step (1), preparing an emulsification kettle with a fractionation device, is provided with a thermometer, a stirrer and a nitrogen inlet pipe in the emulsification kettle;
[0058] Step (2), successively drop into graphene oxide 5g, isomerized tridecyl alcohol polyoxyethylene ether (EO number is 8) 15g, high-density oxidized polyethylene wax 25g, 5g stearyl alcohol, 49.8g water and potassium hydroxide 0.2 g;
[0059] Step ...
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