Insulating and heat conduction material for power battery of new-energy vehicle and preparation method of insulating and heat conduction material
A new energy vehicle and power battery technology, applied in the field of composite materials, can solve the problems of poor material performance stability, unenvironmental use, safety hazards, etc., to achieve excellent mechanical properties, better thermal conductivity, and avoid oxidation effects.
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[0030] Example 1
[0031] A method for preparing an insulating and thermally conductive material for a power battery of a new energy vehicle includes the following preparation methods:
[0032] Step S1 Preparation of intermediate product: under nitrogen atmosphere, add 100g of tetrahydrophthalimide and 113g of diethylstilbestrol into a three-necked flask equipped with a reflux condenser and an electric stirrer, and then add dimethylene 1000g of sulfone, reflux and stir for reaction at 120°C for 10 hours, and then rotate to remove the solvent to obtain an intermediate product;
[0033] Step S2: Phthalimide-based fluorine-containing fluorene polycondensate: 150g of 2,7-dibromo-9,9-difluorofluorene, 100g of intermediate product, and 40g of cesium carbonate are added to a three-necked bottle connected to a water separator , Then add 1000g of dimethyl sulfoxide and 400g of toluene, heat the reaction system to 110°C, stir and react for 3 hours under the protection of nitrogen, remove the ...
Example Embodiment
[0038] Example 2
[0039] A method for preparing an insulating and thermally conductive material for a power battery of a new energy vehicle includes the following preparation methods:
[0040] Step S1 Preparation of intermediate product: under helium atmosphere, add 100 g of tetrahydrophthalimide and 113 g of diethylstilbestrol into a three-necked flask equipped with a reflux condenser and an electric stirrer, and then add N, 1100 g of N-dimethylformamide, reflux and react with stirring at 122°C for 10.5 hours, and then the solvent was removed by rotary evaporation to obtain an intermediate product;
[0041] Step S2: Phthalimide-based fluorine-containing fluorene polycondensate: 150g of 2,7-dibromo-9,9-difluorofluorene, 100g of intermediate product, and 43g of sodium hydride are added to a three-necked flask connected to a water separator , Add 1100g of dimethyl sulfoxide and 450g of toluene, heat the reaction system to 113°C, stir for 3.5 hours under the protection of nitrogen, re...
Example Embodiment
[0046] Example 3
[0047] A method for preparing an insulating and thermally conductive material for a power battery of a new energy vehicle includes the following preparation methods:
[0048] Step S1 Preparation of intermediate product: under a neon atmosphere, add 100 g of tetrahydrophthalimide and 113 g of diethylstilbestrol to a three-necked flask equipped with a reflux condenser and an electric stirrer, and then add N- to the flask. 1,300 g of methylpyrrolidone, reflux and react with stirring at 125°C for 11 hours, and then rotate to remove the solvent to obtain an intermediate product;
[0049] Step S2: phthalimide-based fluorine-containing fluorene polycondensate: 150g of 2,7-dibromo-9,9-difluorofluorene, 100g of intermediate product, and 50g of potassium tert-butylate are added to the water separator In a three-neck flask, add 1300g of dimethyl sulfoxide and 500g of toluene, heat the reaction system to 115°C, stir and react for 4 hours under nitrogen protection, and remove ...
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