Unlock instant, AI-driven research and patent intelligence for your innovation.

Manufacturing method and application of amorphous carbon film on surface of flexible substrate and with both piezoresistance performance and toughness

A flexible substrate and amorphous carbon film technology, applied in ion implantation plating, metal material coating process, coating, etc., can solve the problems of difficult mass production, less application of flexible sensors, and high cost, and achieve good toughness, The preparation is simple and the effect of improving the piezoresistive coefficient

Active Publication Date: 2019-08-30
NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI
View PDF7 Cites 4 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The most representative piezoresistive sensitive material is single crystal silicon, but due to the preparation process, its application in the field of flexible sensors is seldom
In recent years, new sensitive materials represented by graphene and carbon nanotubes have been used more and more in flexible strain sensors. However, due to the transfer process still required after their preparation, their production is difficult to batch and the cost is high.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Manufacturing method and application of amorphous carbon film on surface of flexible substrate and with both piezoresistance performance and toughness
  • Manufacturing method and application of amorphous carbon film on surface of flexible substrate and with both piezoresistance performance and toughness
  • Manufacturing method and application of amorphous carbon film on surface of flexible substrate and with both piezoresistance performance and toughness

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] In this implementation example, the flexible base material is PI, and an amorphous carbon film is prepared on the surface of the flexible base, as follows:

[0039] (1) The flexible substrate is ultrasonically cleaned with acetone and dried, then placed in a vacuum coating chamber and evacuated to 2.7×10 - 3 Pa, then etched the substrate surface with argon plasma for 30min;

[0040] (2) Adopt high-power pulse magnetron sputtering technology, select high-purity graphite target, sputter carbon atoms from the high-purity graphite target through ionized argon gas, and deposit on the surface of the flexible substrate after step (1) Amorphous carbon film, the pressure of argon gas in the vacuum coating chamber is controlled to 0.1Pa, the high-power pulse power supply voltage is 800V, the pulse duty ratio is 1%, and the flexible substrate DC pulse negative voltage is -10V to obtain an amorphous carbon film.

[0041] The above-mentioned flexible substrate deposited on the sur...

Embodiment 2

[0063] In this implementation example, the flexible substrate is the same as in Example 1, and an amorphous carbon film is prepared on the surface of the flexible substrate, as follows:

[0064] (1) is identical with the step (1) in embodiment 1;

[0065] (2) is basically the same as step (2) in embodiment 1, and difference is that the high-power pulse power supply voltage is 1000V;

[0066] Similar to Example 1, the above-mentioned flexible substrate deposited on the surface of the amorphous carbon film was stretched and deformed to test the piezoresistive properties of the amorphous carbon film, and the results were as follows Figure 5 It is shown that the amorphous carbon film has good piezoresistive properties. Similar to Example 1, after the piezoresistive test, the amorphous carbon film did not crack due to the deformation test, and had good toughness.

Embodiment 3

[0068] In this implementation example, the flexible substrate is the same as in Example 1, and an amorphous carbon film is prepared on the surface of the flexible substrate, as follows:

[0069] (1) is identical with the step (1) in embodiment 1;

[0070] (2) is basically the same as step (2) in embodiment 1, and difference is that the pulse duty cycle is 5%;

[0071] Similar to Example 1, the above-mentioned flexible substrate deposited on the surface of the amorphous carbon film was stretched and deformed to test the piezoresistive properties of the amorphous carbon film, and the results were as follows Image 6 It is shown that the amorphous carbon film has good piezoresistive properties. Similar to Example 1, after the piezoresistive test, the amorphous carbon film did not crack due to the deformation test, and had good toughness.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention provides a manufacturing method of an amorphous carbon film on the surface of a flexible substrate and with both piezoresistance performance and toughness. According to the manufacturingmethod, the high-power pulse magnetron sputtering technology is adopted, a graphite target is selected, the amorphous carbon film is formed on the surface of the flexible substrate in a sputtering deposition mode in the inert gas atmosphere, the voltage of a pulse power source ranges from 800V to 1000V, and the pulse duty ratio ranges from 1% to 5%. Compared with the prior art, the manufacturingmethod has the advantages that the phenomenon that due to the fact that the temperature is overhigh in the manufacturing process, a flexible substrate material is destroyed is also avoided, and therefore the amorphous carbon film can be applied to a flexible piezoresistance sensing element, and the flexibility of the piezoresistance sensing element is achieved.

Description

technical field [0001] The invention belongs to the technical field of piezoresistive sensors, in particular to a preparation method and application of an amorphous carbon film with piezoresistive performance and toughness on the surface of a flexible substrate. Background technique [0002] In recent years, flexible strain sensing devices have been widely used in wearable devices, robots, biomonitoring, etc. The performance of the sensor is mainly determined by the sensitive material, and the piezoresistive sensitive material is a widely used sensitive material. An important parameter to characterize the performance of piezoresistive sensitive materials is the piezoresistive coefficient, which reflects the sensitivity of piezoresistive materials. [0003] The most representative piezoresistive sensitive material is single crystal silicon, but due to the reason of preparation process, its application in the field of flexible sensors is seldom. In recent years, new sensitiv...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C23C14/35C23C14/06C23C14/04
CPCC23C14/042C23C14/0605C23C14/3485C23C14/35
Inventor 汪爱英马鑫郭鹏张栋赵玉龙张琪
Owner NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI