Nanostructure-containing polycrystalline diamond, polycrystalline diamond composite sheet and preparation method thereof
A polycrystalline diamond and nanostructure technology, applied in nanotechnology, metal processing equipment, transportation and packaging, etc., can solve the problems of lack of strong bonding, overcome the difficulties in the preparation process, improve the comprehensive mechanical properties of hardness and toughness, The effect of overcoming cleavage brittle fracture
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[0051] Example 1: Preparation of nanostructure-containing polycrystalline diamond
[0052] Commercially available Kabuna polytype nanostructured polycrystalline diamond particles and microscale single crystal diamond particles are used as raw materials for synthesizing polycrystalline diamond. The cabuna polytype nanostructured polycrystalline diamond particles are synthesized by the blast shock wave method, and they contain 99.0% to 99.5% (weight percent) of diamond, and have a nominal size of 10 microns and are in the form of lumps. Micron-scale single crystal diamond particles were synthesized by static HPHT method, and they contained 99.5 wt. % diamond with a nominal size of 10 microns and were in the form of lumps. The two diamond particles were mixed in a mass ratio of 1:1. These diamond particles are treated with high temperature alkali and acid solution to further remove impurities. High temperature alkali solution treatment is to mix diamond particles with sodium hy...
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[0053] Example 2: Preparation of nanostructure-containing polycrystalline diamond compacts
[0054] Commercially available Kabuna polytype nanostructured polycrystalline diamond particles and microscale single crystal diamond particles are used as raw materials for synthesizing polycrystalline diamond. Kabuna polytype nano-structured polycrystalline diamond particles are synthesized by an explosion shock wave method, and they contain 99.0% to 99.5% (weight percent) of diamond, and have a nominal size of 10 microns and are in the form of lumps. Micron-scale single crystal diamond particles were synthesized by static HPHT method, and they contained 99.5 wt. % diamond with a nominal size of 10 microns and were in the form of lumps. These diamond particles are treated with high temperature alkali and acid solution to further remove impurities. High temperature alkali solution treatment is to mix diamond particles with sodium hydroxide (NaOH) in a mass ratio of 1:5, heat to 500°C ...
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[0056] Example 3: Preparation of nanostructure-containing thermally stable polycrystalline diamond and nanostructure-containing thermally stable polycrystalline diamond compacts
[0057] In this example, the samples used in the test are the polycrystalline diamond containing nanostructures in Example 1 and the polycrystalline diamond compacts containing nanostructures in Example 2. The metal binder-cobalt is removed with a mixed acid. The volume composition of the mixed acid is: 25% nitric acid (concentration of 95wt.%) and 75% hydrochloric acid (concentration of 36wt.%), and the decobalt depth is about 0.2 mm. Prepared separately A thermally stable polycrystalline diamond containing nanostructures and a thermally stable polycrystalline diamond compact containing nanostructures are produced.
[0058] In the present invention, the preparation method of nanostructure-containing polycrystalline diamond and polycrystalline diamond composite sheet is similar to the preparation meth...
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